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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample 9/17 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Heptadecanol Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 29.78 0.58 ug/1 90531 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qu al

1 1-Heptadecanol 256 C17H36O 001454-85-9 93 2 1-Octadecanol 270 C18H38O 000112-92-5 93 3 4-Tetradecanol 214 C14H30O 001653-33-4 81 4 1-Nonadecanol 284 C19H40O 001454-84-8 76 Abundance Scan 2695 (29.783 min): LBD.D (-) m/z 43.05 100.00% 4)3

83 55 69 97 5000 / 111 J940_2a60_ja80_3a00_30^ ' ' I ' Wz 83705 61.97% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #35210:1-Heptadecanol 55 69 83 97 553 l{K/\ I''' 'I'' ‘' I 111 29.40 29.60 29.80 30.00 30.20

■n/z~> Abundance 40 60 80 ux 100 125

120 140 #72029:1-Octadecanol 160 ................. 210.......... 238 180 200 220^240 T m/z55.00 54.21%

43 56 69 83 .................... 97 29 40 29.60 29.80 30.00 30.20 5000 m/z 60795 51.81% 111 125

■n/z-> ' ' I ' ' 40 60 ' ' I' 80 X UI 100 120 ................................................ 224 140 160 180 200 220 240 252

MA Abundance #26420: 4-Tetradecanol 43 _294g_^a60_2a80_3qw_3g^ 57 m/z 57.00 51.49% 83 97 5000 70 111 125

■n/z-> 40 60 80 - 100 I 120 140 /86 160 180 196 200 220 240 XU ' ' I ' . . I I Ti , , I I 29.40 29.60 29.80 30.00 30.20

LBD.D NP091101.M Tue Oct 02 12:28:36 2001 Page 9

NYC-WTC_000086995

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NYC-WTC_000086995Source: NYC Law Department, mirrored locally

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