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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086994
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT0101\LBD. D Vial: 4 Acq On : 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample ; 9/17 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Tetracosane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 29.65 0.89 ug/1 139452 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 90 2 Heptadecane 240 C17H36 000629-78-7 90 3 Octadecane 254 C18H38 000593-45-3 90 4 Pentacosane 352 C25H52 000629-99-2 90 Abundance Scan 2681 (29.654 min): LBD.D (-) m/z 56.95 100.00%

43 71 ft 95S 85

n/z-> 40 y 60 J, Ji, iJ „| ^1155169183 211 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I'''' I'''' I'''' I'''' I' 29.40 29.60 29.80 30.00 m/z 71.05 75757% Abundance #73543: Tetracosane 43 5l7 71

5000 85 .. J y/Lgs.. 29.40 29.60 29.80 30.00 . m/z 43700 64.86% J j227 155169183197 _________ 294 I'' ‘' I'' '' I'''' I 338 I' ‘' I' (1 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71194: Heptadecane 4(3 57 A 29.40 29.60 29.80 30.00 71 5000 m/z 85.05 45.07% 85 A T P127141155169183 212 240 TTpT I ' ' ' ' I ' I'''' I'''' I' ''' I' ' I '''' I'' ’' I'''' I'' ‘' I'''' I'''' I'''' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71559: Octadecane 43 5(7 29.40 29.60 29.80 30.00 m/z 41700 26.88% 71 5000 85

T ^‘{^'’27141155169183 226 254 ' I'''' r ''' I' p-r-r-q-T-rrry p-TT-q-m-T-p pi, , I 1 , . , I ■n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 29.40 29.60 29.80 30.00

LBD.D NP091101.M Tue Oct 02 12:28:32 2001 Page 8

NYC-WTC_000086994

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NYC-WTC_000086994Source: NYC Law Department, mirrored locally

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