GCMS sample analysis AD29285, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29293.D Vial: 14 Acq On 12 Dec 2001 3:40 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Chrysene-dl2 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.01 25.70 ug/l 5038290 Perylene-dl2 37.09

Hit# o 5 Tentative ID MW MolForm CAS# Qual

1 Ch ysene-dl2 240 C18D12 001719-03-5 98 2 1,7 -Bis(6-methylpyridyl -3)-butane 240 C16H20N2 000000-00-0 50 3 Alizarin 240 C14H804 000072-48-0 47 4 Naphtho[2,1-b:7,8-b']difuran, 1,2,9 240 C16H1602 068873-21-2 43 Abundance Scan 3046 (33.008 min): 29293.D (-) m/z 240.15 100.00% 240

5000 - i ------ . I 120 1 । • • ■ ■ । > 106 32.60 32.80 33.00 33.20 33.40 42 52 66 78 92 l| J 132 146156 170180 194 212222 , 0 TI————dm—dtor 4—r TII—TTvmt all . m/ z 23 6.05 23.78% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance . #32068: Chrysene-d12 240

5000 - 32.60 32.80 33.00 33.20 33.40 m/z 239.15 22.34% 106 120 I ,1.11.... 156...... 212 m/z-> 40 60 80 100 120 140 160 180 200 220 240 'Abundance #32046: 1,4-Bis(6-methylpyridyl-3)-butane 240 1 TEEE101 107 l i ' ■ ' ■ i ' I 32.60 32.80 33.00 33.20 33.40 5000 m/z 120.05 19.12% 77 120 134 39 51 ■ i ■ ■ ' 65 ; ll 92 I i m/z-> 40 60 80 100 120 140 160 180200 220 240 Abundance #31937: Alizarin i ■ ■ ■ ■ i ' ■ i ' 1 i 1 1 1 1 1 1 1 240 32.60 32.80 33.00 33.20 33.40 m/z 241.15 18.80% 5000

128138 184 212 76 92 159 194 1 — I TT - — 1 1 I 1 1 ' 1 I m/z--> 40 60 80 100 120 140 160 180 200 220 240 32'eO 32.8QT~33.00 33.20 33720

29293.D GCMS1126.M Fri Dec 28 15:24:41 2001 Page 5

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