GCMS sample analysis AD29285, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29293.D Vial: 14 Acq On : 12 Dec 2001 3:40 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Bis(2-ethylhexyl) phthalate Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

33.29 0.60 ug/1 116755 Perylene-dl2 37.09

Bit# of 5 Tentative ID MW MolForm CAS# Qual

Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 91 2 1,2-Benzenedicarboxylic acid, 3-nit 211 C8H5NO6 000603-11-2 86 3 Di-n-octyl phthalate 390 C24H3804 000117-84-0 59 4 1,2-Benzenedicarboxylic acid, butyl 304 C18H24O4 _________ 000084-64-0 53 Abundance Scan 3077 (33.292 min): 29293.D (-) m/z 149.00 100.00%| 149

5000 57 167 43 ‘ 8 rrrrrrr| T . 71 83 _ 113 279 33.00 33.20 33.40 33.60 || — 97 +44 r 132 L r, p 207 I ! I I I I ' 11 ' I 1 ; : —-rrripT-s—-pr m/z 167.00 31.07% m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53128: Bis(2-ethylhexyl) phthalate 149

5000 A 57 167 33.00 33.20 33.40 33.60 71 m/z 57.00 26.83% 83 113 279 — 132 | 1 • > i • ■ • 1 i • miz-> ' 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25513: 1,2-Benzenedicarboxylic acid, 3-nitro- 149 > • i > ■ ■ ' i ' ' ■ ' i ■ 33.00 33.20 33.40 33.60 5000 - m/z 71. 16.18% 167 71

■ ■ i ' ■ ' ' i ' .1 83 । i 113 132 ' I • m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #74175: Di-n-octyl phthalate A AAAALA— 149 33.00 33.20 33.40 33.60 m/z 42.95 15.95% 5000

57 7183 104 121 167 261 279 m/z-> ...... 40 4 60 1111—1111—— .,, TTOr 1TT1-1—00T1B0B——mTTTT 80 100 120 140 160 180 200 220 240 260 280 33. 33.20 33.40 33.60

29293.D GCMS1126.M Fri Dec 28 15:24:46 2001 Page 6

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