GCMS analysis results for sample AD31405, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 602\31405.D Vial: 11 Acq On : 16 Jan 2002 9:25 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Dibutyl phthalate Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

26.80 0.23 ug/1 69681 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1(ibutyl phthalate D 278 C16H2204 000084-74-2 90 2 Bis(2-methoxyethyl) phthalate 282 C14H1806i 000117-82-8 83 3 1,2-Benzenedicarboxylic acid, dipro 250 C14H1804 000131-16-8 78 4 1,2-Benzenedicarboxylic acid, butyl 304 C18H24O4 000084-64-0 78 Abundance Scan 2370 (26,800 min): 31405.D (-) m/z 149.00 1 00.00% 149

5000

26.40 26.60 26.80 27.00 27.20 93 104 121 76 , 11 ,, 411 rh"561 Pi rP aimaag । 188 205 223 ■ ■ 1 ■ • ■ ■ i ■ 1 ■ ■ i ■' 1 ■ ■ i '■ • • ■ i ■ ■ TT-p-T-TT-p- m/z 150.00 9.10% miz-> 40___ 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72214: Dibutyl phthalate 149

5000 26.40 26.60 26.80 27.00 27.20 m/z 41.05 8.93% 41 56 76 93 104 121 205 223 278 •' ।1 -r-r+pn-r+pr 1 • i *'1 ‘ ■ T' ‘ ■ i • ' 1 ‘ i ‘ ■ i ■ ‘ ‘ • i * ■ ‘ ■ i ■ ■ ■ ■ i • ■ ■ ■ i • ■ ■ ' i ' miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39720: Bis(2-methoxyethyl) phthalate 149 vaprwakoin/ Uorrun 26.40 26.60 26.80 27.00 27.20 5000 m/z 56.0,0 5.63%

41 ™ 57 76 93 104 121 160 205 223 • • i 1 ' ‘ ' i ■ ■ ‘ ■ i 1 ' 1 ■ i ' ‘ ■ i • i ■ ■ ■ ■ i ' 1 ■ 1 i ■ • ■ • i' ' ■ ■ i ■ ■ ■' i ■ • ' ■ i • 1 ■ ■ i ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71449:1,2-Benzenedicarboxylic acid, dipropyl ester 149 26.40 26.60 26.80 27.00 27.20 m/z 103.9,5 5.43% 5000

43 65 76 93 104 121 , 101 209 miz-> Maahaju) 1 11" l‘l I p' 1 1 1 | merHii I |‘'l l 1 I | I ti | IT 40 60 80 100 120 140 160 180 200 220 240 260 280 26.40 26.60 26.80 27.00 27.20 250 • ' i • ' 1 ' i ' ‘ ‘ ‘ i ‘ ‘ 1 ( ■

31405.D GCMS0103.M Thu Feb 07 09:14:40 2002 Page 4

NYC-WTC_000018383