GCMS analysis results for sample AE01691, March 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2502\1691.D Vial: 12 Acq On : 25 Feb 2002 10:21 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Bis(2-methoxyethyl) phthalate Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

27.68 0.24 ug/1 22902 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bis(2-methoxyethyl) phthalate 282 C14H1806 000117-82-8 83 2 Dibutyl phthalate 278 C16H2204 000084-74-2(83 3 Phthalic acid, butyl ester, ester w 336 C18H24O6 000085-70-1 83 4 1,2-Benzenedicarboxylic acid, bis (2 278 C16H2204 000084-69-5 78 Abundance Scan 2466 (27.679 min): 1691.D (-) 149 m/z 149.00. 100.00%

5000 ' ■ i • ' ■ 1 i ■ ■

41 56 76 93 104 121 205 223 27.40 27.60 27.80 28.00 1mt IF+4I "i * ■ * ■ । । । ■ 1 11144****I*’I* m/z 150.00 9.20% miz-> _ 40. .60 80 100. 120 140 160 180 200 220. 240. 260.280 Abundance #39720: Bis(2-methoxyethy!) phthalate 149

5000 27.40 27.60 27.80 28.00 41 m/z 41. C 5 7.90% 160 205 223 • • ।1 57 .. 76 . 93 104 121 . 160 180 200 " 220 240 260 280 mz-2___ 40 60 80 100 120 140 Abundance 149

27.40 27.60 27.80 28.00 5000 m/z 56.00 5.36%

41 56 76 93104 121 205 223 278 ■ • i • m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #73511: Phthalic add, butyl ester, ester with butyl glycol 149 27.40 27.60 27.80 28.00 m/z 103.85 4.76% 5000-

57 76 93 104 121132 205 223 Il t P2919tdt—310ma11 160 278 —9*1mTTT ‘ * I ’ ‘ ‘ * 1 * m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 27.40 27.60 27.80 28.00

1691.D GCMS0208.M Thu Feb 28 09:34:02 2002 Page 2

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