GCMS analysis results for sample AD31341 with surrogate data, Feb

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB0802\31341.D Vial: 25 Acq On 9 Feb 2002 8:39 am Operator: 209 GALOS Sample RE-EXTRACT 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Dibutyl phthalate Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

27.71 0.22 ug/1 26629 Phenanthrene-dl0 25.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dibutyl phthalate _ 2 78 C16H2204 000084-74-2 83 2 1,2-Benzenedi carboxyli c acid, dipro 250 C14H1804 000131-16-8 78 3 1,2-Benzenedicarboxylic acid, butyl 278 C16H2204 017851-53-5 74 4 1,2-Benzenedicarboxylic acid, butyl 304 C18H24O4 100.00% 74 000084-64-0 Abundance Scan 2469 (27.712 min): 31341.D (-) m/z 149.00 1 9

5000

41 27.40 27.60 27.80 28.00 l ■ " ' 'I1" 56 76 104 — t121 205 223 r • * • • । • • • > । • •«* । •1 * -1 "1 ■' i ■ ■ 1 1 i 1 ' 1 ' 1 1 1 1 1 1 1 m/z 41.05 12.02% m/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72214: Dibutyl phthalate 149

5000 27.40 27.60 27.80 28.00 m/z 150.00 7.86% ........................................................... .. 223 .. ............ m/Z->__ 20 40 60 __ 80 100 120 140 160 180 200 220 240 260 280 Abundance . •< i 1 1 .. 9 “0 2 0 149

27.40 27.60 27.80 28.00 5000 m/z 103.95 6.28%

43 56 76 104 121 191 209 250 m/z-> 20...... 40 60 80 .. 100 120 140 160 180 200 220 240 260 280 Abundance #39131:1,2-Benzenedicarboxyiicacid, butyl 2-methylpropyl 149 27.40 27.60 27.80 28.00 ' ' ' m/z 56.00 5.66% 5000

27 41 57 76 104 205 223 i ' ■ ‘ 1 i ■ ' 1 ' i T '121 278 1 ‘ । I | i . , ■ | > i . I | I I I I | CUTFTl ! I I | I I I I 11—74’1 I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 27.40 27.60 27.80 28.00

31341.D GCMS0208.M Thu Feb 14 15:03:26 2002 Page 3

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