GCMS analysis results for sample AD31341 with surrogate data, Feb

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB0802\31341.D Vial: 25 Acq On 9 Feb 2002 8:39 am Operator: 209 GALOS Sample RE-EXTRACT 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxypropox Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.27 0.43 ug/1 41434 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 7-------------------- 1 2 - Propane. , 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 74 2 2-Propand 1- [l-methyl-2-(2-propen 174 C9H18O3 055956-25-7 40 3 1,2-Dideoxy-l-erythro-pentitol 120 C5H12O3 000000-00-0 39 4 Hexylene Glycol 118 C6H14O2 000107-41-5 38 Abundance.. ..... . Scan 787 (12.271 min): 31341.D (-) m/ z 59 5000 / 45 __ 12.00 12.20 12.40 12.60 39 1 1 ' 1 1 1 '‘,I 73 84 104 m/z 4’5 0 5”.. 17.99%

_NA m/z-2 20 30 40 50 (60 70 80 90 100 110 120 130 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59

5000 ■ ■ i ' ' ____ 12.00 12.20 12.40 12.60 m/z 43.05 16.05% 31 45 ' I ' ' ' ' I' rH ;..... 73.................. 104.............. 130 ' I ■ ' ‘ ' i ' ' ■ ■ i ' ' ' ' 1 1 ■ ' ' i ' 1 ' ' i ■ ■ ■ ' i ‘ ' i ■ m/z—20 30 40 50 60 70 80 90 100 110 120 130 Abundance 59 M.--A- ____ 12.00 12.20 12.40 12.60 5000 m/ z 41.05i 14.92% 103 31 45 73>85 117 130 TO00OB—mnnB—B————-IB/m——Bn=-n/mmTmmTTTRTTTTTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 44 #3714: 1,2-Dideoxy-l-erythro-pentitol 59 —MP— 12^00 12:20 1240 12.60 m/ z 42.05 11.14% 31 5000

m/z~> —IT 20 30 1 ■ i ■ 40 T-r-p-r 50 71 89 h ■'' ■ J1'1'1111 ■ ''1111 ■ । ■1 ■' । ■11 ‘ । ■ ■ ■ ■ ।'' 60 70 80 90 100 110 120 130 M12.00 12.20 12.40 12.60

31341.D GCMS0208.M Thu Feb 14 15:03:22 2002 Page 2

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