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GCMS analysis results for sample AD31341 with surrogate data, Feb

Machine-extracted title · confidence 50%

Laboratory report for sample AD31341 showing GCMS analysis of unknown compounds and surrogate recovery on February 15, 2002.

NYC-WTC_000003880–000003890

Folder label: “GCMS X 1/28/02 A 2/8/02

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Scanned page image, NYC-WTC_000003887
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\1\DATA\FEB0802\31341.D Vial: 25 Acq On 9 Feb 2002 8:39 am Operator: 209 GALOS Sample RE-EXTRACT 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.05 0.30 ug/1 28993 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol -(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 64 2 Ethane, 1- hoxy-l-methoxy- 104 C5H1202 010471-14-4 40 3 2-Pentanon 5-methoxy- 116 C6H1202 017429-04-8 33 4 2-Propanol 1,1' -oxybis- 134 C6H14O3 000110-98-5 28 Abundance f Scan 763 (12.050 min): 31341.D(-) m/z 59.05 100.00% 59 45

5000 103 / 73 39 ' 1 i ' ' 1 ■ i ' ' 11.80 12.00 12.20 12.40 -'i11''i'1''i'1'■i'1''i''1‘i'1 1111 , 84 । ■ I ■ 1 ■ 1 1 1 m/z 44.95 66.42% miz- 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 11.80 12.00 12.20 12.40 73 31 m/z " 38.52% —PTP-Tm । ■ ■ i ■ ■ ' ■ i - ■ । 130 ■ i ■ ■ m/z->20 30 40___ 50 60 70 80 90 100 110 120 130 Abundance

45 59 M), 11.80 12.00 12.20 12.40 5000 m/ z 73.00 3 .43% 73 89 27 ............................... .................. 103....................................

..... MM.., 1 । ‘ 1 ■ ■ । 1 ■ ■ ' । 1 ■ m/z-? _ 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64282: 2-Pentanone, 5-methoxy- 43 59 11.80 12.00 12.20 12.40

. AA, m/ z 41.05 35.37% 5000

69 | , 84 101 116 ' I ' ' ' ' I ' ' ' ' I1 > l . I . . IIannnIunn-nIaIaIIanv i 1 111 4 41 I I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 11.80 12.00 12.20 12.40___

31341.D GCMS0208.M Thu Feb 14 15:03:17 2002 Page 1

NYC-WTC_000003887

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NYC-WTC_000003887Source: NYC Law Department, mirrored locally

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