GCMS analysis comments for sample AD29139, Dec 17 2001

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29139.D Vial: 11 Acq On : 10 Dec 2001 8:30 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.62 ug/1 151076 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID.” MW MolForm CAS# Qual

1 2-Propanol, l-(2-j thoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3‘-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Pentanone, /5-methoxy- 116 C6H1202 017429-04-8 53 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance 7 Scan 696 (11.430 min): 29139.D (-) m/z 59.05 100.00% 59

5000 45 103 73 I ‘1 1 11'1 * i * * * • i * * r• i * • 11.00 11.20 11.40 11.60 11.80 - 1i>'1'i1‘1 ‘' m/z 44.95 43.46%

N m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 TIT T T T T 45 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.00 34.65% ....... 4................... 130........ — TTTTTutIr miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859; 2-Butencl, 2 3‘-pxybis- 59 1 ■ —4+ -T T 11.00 11.20 11.40 11.60 11.80 5000 31 m/z 73.0,0 28.21%

NJ 45 103

— ■ 4—— - •i ■■■■ 134 • 1 ■ i ■ ■ • • i • • ■ ■ i ■ ■ ■ ■i11■■I 1■■■i•■••i•■■11‘ miz-? 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #64282: 2-Pentanone, 5-methoxy- I -^i ■ ' T T 43 59 11,00 11.20 11.40 11.60 11.80 m/z 41.05 17.25% 5000

m/z-> 11 ■ • ■ • । • 20 30 '1111111' 40 50 60 69 1—I, 84 । 70 80 90 ‘ 101 । ■ • ■ ■ । 100 110 116 •1 ■ । 120 ‘ ।' 130 ।' 140 N 11.00 11.20 1140 11.60 11.80

29139.D GCMS1126.M Wed Dec 12 16:07:15 2001 Page 4

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