GCMS analysis comments, sample AD28970, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 701\28970.D Vial: 15 Acq On 8 Dec 2001 4:35 am Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.60 ug/1 156645 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-1methoxy- 1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3-oxybis- 162 C8H18O3 054305-61-2 50 3 1-Propanol, 2- (2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45

A 4 2-Pentanone,^5-methoxy- 116 C6H1202 017429-04-8 42 Abundance Scan 696 (11.431 min): 28970.D (-) m/z 59.05 100.00% 59 5000 45 73 103 11.20 11.40 11.60 11.80

m/z-> 39 il ■ i ■ ■1 ■ । '1 +11 Ptt 20 30 40 50 60 70 80 -H i • • ■ ' I 1 • ■ ■ i ■ ■ 1 ■ i ■ 90 100 110 120 130 140 m/z 45.05 44.51% Abundance #9238: 2-Propanol, 12-methoxy-1-methylethoxy)

5000 T111r ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • 45 103 11.20 11.40 11.60 11.80 73

. tL 31 m/z 73.0,0 31.16% 1 1 1 1 • > — ----- .......... ।......... 130.... miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3.3’-oxybis- 59 11.20 11.40 11.60 11.80 5000 31 45 m/z 102.95 31.13% 103

! ,!..... .................. i........... 134,,, —TTauuaagi‘1 • • i • • • • i • • • • i1 • ‘ • i • • • • I • ‘ • i1 ■ ■ • i • • • • i ■ ■ • ■ i ■ • • • i1 miz-> 20 30 40I 50 60 70 80 90 100 110 120 130 140 Abundance #6086:1-Propanol, 2-(2-hydroxypropoxy)- TIfeur ' i * ■ TTPr 4 * 59 11.20 11.40 11.60 11.80 m/ z 41.05 24.39%

m/z—> 5000 31 45

TPPPT — II + 1 । r r rHTr 11175 20 30 40 50 60 70 89 TTTIT। .'i.. t.... j.... j।. 80 90 100 110 120 130 140 103 NU CMY 4 4M . I .... 1 .... 1 .> 11.20 11.40 11.60 11.80

28970.D GCMS1126.M1 Thu Dec 13 10:29:52 2001 Page 3

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