GCMS analysis comments, sample AD29233, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29233.D Vial: 15 Acq On : 11 Dec 2001 12:23 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.41 3.72 ug/1 1139480 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol , 3,3’ -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 4 2-Pentanol, 2-methyl- 102 C6H140 000590-36-3 42 Abundance Scan 694 (11.413 mln): 29233.0 (-) m/z 59.05 100.00%

5000

39, —menntH 45

41—5053 460... 70r 73

89 । teT TIT mr । . 1. ■ 103

130 . . • ‘ I ‘ ‘ ‘ ‘ I 1 1 1 1 I ‘ i ■ 1 ■ • i ■ ■ M 11.00 11.20 11.40 11.60 11.80 m/ Z -----

m/z-> 20 30 401 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(J . - 59

5000 103 TTI 45 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 37.43%

V —Pne .................... ,.................... 130......... »i •.. • । • 11’ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3-oxybis- 59 — * — * . 1 ’ft ‘ 11.00 11.20 11.40 1160 11,80 5000 31 m/z 73.00 28.24%

UA 45 103

1________________ 134 ■ i • ■ i ■ ■ ‘ • i ‘ 1 ■ i ■ ■ ‘ ■ I ■ ■ 1 ■ i • ' ■ • i • ■ • ■ i ■ ■ • ■ i ■ ■ • ■ i ■ ■ h • i • • ■ ■ i ■ ■ ■ ■ i ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- I ’ • r ‘ l ’ ' 59 11.00 11.20 11.40 11.60 11.80 m/z 41.05 24.21% 5000

m/z—> 31 --------------- Sii 73 45 ............. 104........... 130 1.8 T I J T I TT 1TTT I TB Ton J 1I TId * * T I * * I I I I 20 30 40 50 60 70 80 90 100 110 120 130 140 JU i ' 1 1 1 1 * 2t - 1 - - 1 $ t t I I I I 1k 11.00 11.20 11.40 11.60 11.80

29233.D GCMS1126.M Fri Dec 14 16:13:07 2001 Page 5

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