GCMS analysis comments, sample AD29233, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29233.D Vial: 15 Acq On : 11 Dec 2001 12:23 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1-Nonadecanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 29.66 0.93 ug/1 222480 Chrysene-dl 2 33.01 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Nonadecanol 284 C19H40O 001454-84-8 93 2 1-Tetradecanol, acetate 256 C16H3202 000638-59-5 83 3 1-Pentadecanol 228 C15H320 000629-76-5 81 4 l-Heptadecanol 256 C17H360 001454-85-9 64 Abundance ’ Scan 2682 (29.664 mln}: 29233.D (-) m/ z 43.05 100.00% 43

55 83 97 5000 69 111 । I ... L 125 139I » *153I I........._ 196207 224 I J l I if 2940 29.60 29.80 30.00 ■ ■ ■ r ■ *4 i TTTTTTTT . TTIm. / I I TTT J T DTnnnpUnTTm 252» J m/z 55.00 54.30% miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #40236: 1-Nonadecanol 55 69 83 97

5000 PPMTTTP 111 29.40 29.60 29.80 30.00 31 42 125 m/ z 83.05 52.92% n fi TTII8 ■ • । * Illi *10*——_—-—C11rouuu—rTe—r—238 111313t mz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #35194: 1-Tetradecanol, acetate __ _ 55 69 83 Tffrr 97 29.40 29.60 29.80 30.00 5000 m/z 57.00 48.90% 111 I, 125 168 196 | 210____________ ’ 1’5-1r1ruT * i • • • • 1’tT । । । » i > । । । T TII T 1T J I I T T IT TTIT m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #70846: 1-Pentadecanol 41 14 TI 4 --=00 A 69 S3 29.40 29.60 29.80 30.00 31 97 m/z 97.05 48.87% 5000 56 111 125 182 210 TTT l ■ ■ ■ • i 1 •r | < i “f.Mr miz-> 40 60 80 100 120 140 160 180 200 220 240TT 29.40 29.60 29.80 30.00

29233.D GCMS1126.M Fri Dec 14 16:13:12 2001 Page 6

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