GCMS analysis comments, sample AD29189, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29136.D Vial: 19 Acq On : 11 Dec 2001 4:17 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.35 1.02 ug/1 202916 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3‘-oxybis- 162 C8H18O3 054305-61-2 50 3 2-Pentanone, 5-methoxy- 116 C6H1202 017429-04-8 45 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance Scan 686 (11.346 min): 29136.D (-) m/ z 59.05 100.00%

4. 59

5000 45 103

miz-? Abundance 20 • i ■ ■ • 1 i 1 30 39111, 40 45501 —H60er70— # 80 85 73 । 90 100 110 120 130” 140 #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) m/z NA 1 ' 1 1 1 ' I ‘ ‘ I ' ■ 1 • I ‘ 1 1 1 > 1 11.00 11.20 11.40 11.60

59

5000 103 T T T T r1 45 73 11.00 11.20 11.40 11.60 31 m/z 103.05. 37.89% — —I TI • । • PT i r ‘ । . । > । । i 11 > ।. I । ■ i • • 1' i ■ ' ■ 130 ■ i • 1 ■ ' i ■ miz-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #12859:2-Butanol. 3,3°-oxybis- 59 T T T T TI1 11.00 11.20 11.40 11.60 5000 31 m/z 73.00 0, 27.49% 45 103

■ m/z-> Abundance 20 is. 134 ——gtaTTTTTTT 30 40.. 50

43 60 70 80 90 100 110 #64282: 2-Pentanone, 5-methoxy- 120_ 130 140 TI_TTTOTTTTT UA 11.00 11.20 11.40 11.60 m/z 3, 41.05 24.61% 5000

miz-> 1 1 1 ‘ ‘ 1 i ■ ■ • ‘ i 1 20 30 40 1 • i 1 ■ 50 60 69 |, 70 80 84 90 101 100 110 116 120 130 140 VA ' I 1 1 1 ' I 1 ' 1 1 I 1 11.00 11.20 11.40 11.60

29136.D GCMS1126.M Fri Dec 14 16:06:32 2001 Page 2

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