GCMS analysis comments, sample AD29189, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29136.D Vial: 19 Acq On : 11 Dec 2001 4:17 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 1.47 ug/1 292288 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 l-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 39 4 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 38 Abundance Scan 695 (11.428 min): 29136.D (-) m/ z 59.05 100.00% 59

5000

<nfz-> 20 Abundance ' 30 40 39.1 45

54

#9238: ’-Propanol, 1-(J 73

84 T1TT 11 I1 —47 - । — 11B——eT—ngr TImuui-WT—Trtr 50 60 70 80 90 100 110 120 130 140 - -- 130 103 A ." W 14." 11.00 11.20 11.40 11.60 11.80

59

5000 103 T T T T T 45 73 11.00 11.20 11.40 11.60 11.80 31 m/z 103.05 33.08% T'1'r t T-rT-p-r-r-T-p- . 130 1 111 7—1——— m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 p ’ • ‘ I ‘ ’ TT ‘ TT T I ‘ ‘ TTrrrf 11.00 11.20 11.40 11,60 11.80 5000

m/z—> Abundance 20 31 45

! 50 75 •p-r-rT-r^T-r-r-p-tVTT-pr-rT^-j-rT-r-p-T-T^^ 30 40 60 70 80 89 90 103

T11r •1 100 #12859:2-Butanoi, 3,3‘-oxybis- 59 • ■ ■1111111 ■ ■ TIT 1 110 120 130 140 m/z

m/ z N 73.00 25.79%

11.00 11.20 11.40 11.60 11.80 1 41.05 20.69% 5000

m/z—> —20P 30 40 31 45

■ ■ TT 1ttr —a—maapppT 50 I60 70 80 134 103

111 TIT 1 , TTT 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80 . NA 29136.D GCMS1126.M Fri Dec 14 16:06:37 2001 Page 3

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