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GCMS blank analysis results for sample AD29932, Dec 2001

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry blank report for sample AD29932 analyzing nitrosamines and chlorinated compounds on December 18, 2001.

NYC-WTC_000037219–000037234

Folder label: “GCMS X 12/11/01 A 12/18/01

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Scanned page image, NYC-WTC_000037233
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC18 01\LB.D Vial: 6 Acq On 18 Dec 2001 8:58 pm Operator: 209 GALOS Sample gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Propanol, 2-(2-hydroxypropox Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.48 ug/1 126093 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propanol, 2-2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 59 2 2-Propanol, -(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 56 3 2-Propane1, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 4 Ethane, -ethoxy-l-met hoxy- 104 C5H12O2 010471-14-4 45 Abundance / Scan 696 (11.430 min): LB.D (-) m/z 59.05 100.00% i / 59

m/z-> 5000

............39 30 I— 40 45

II I4 i— +. '-’-’-I-' 50 160 70 73

78 80 86 90 103

100 110 120 130 11.00 m/ z N 11.20 11.40 11.60 11.80 45.0.5 54.10% Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59

5000- --IPI 31 11.00 11.20 11.40 11.60 11.80 45 103 m/z 102.9 30.31% 75 89 FT ' 1 Tr. '■’■'T ' ' ' i • ' ' ' I ' 1 TIIdnn T~ ' ' ‘ 7 ' m/z-> 30 40 50 60 I 70 80 90 100 110 120 130 Abundance #9238: 2-Propanol, 1-(2-rnethcxy-1-niethylethoxy)- 59 A TII 11.00 11.20 11.40 11.60 11.80 5000 - m/ z 41.05 29.03%

N 45 103 73 31 II , . i I 130 ■ । ■ • ■ • । > i • ■ i ' ■ ' ■ i ' ' rn/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy) TMAAr 59 11.00 11.20 11.40 11.60 11.80 m/z 73.00 5.71%

m 5000-

31 ----- 30 40 45

50 60 70 73 80 90 104 100 110 120 130 130 N Tdn—nCm—nnmm—nm 11.00 11.20 11.40 11.60 11.80

LB.D GCMS1126.M Tue Jan 15 15:41:16 2002 Page 3

NYC-WTC_000037233

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NYC-WTC_000037233Source: NYC Law Department, mirrored locally

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