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GCMS analysis results for sample AD26827, Dec 21 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26827 identifying unknown compounds on December 21, 2001.

NYC-WTC_000032160–000032171

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\26827.D Vial: 11 Acq On : 27 Dec 2001 9:53 pm Operator: 209 GALOS ' Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.48 ug/1 158190 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-l-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1‘-[(1-methyl-1,2-eth 192 C9H20O4 001638-16-0 50 3 2 - Propanol , 1,1' -oxybis- 134 C6H14O3 000110-98-5 36 4 Ether / 74 C4H10O 000060-29-7 36 Abundance Scan 697 (11.440 min): 26827.D (-) m/ z 59.05 100.00% 59 45 5000- 73 103 T TTT ————————— 1-T

miz-> 20 l 30 40 4—T --- 50 60 7G 80 90 100 110 83............. 4......................... 120 130 m/z 11.20 11.40 11.60 11.80 45.00 59.90% Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy)- 59

5000 45 103 4 73 11.20 11.40 11.60 11.80 31 m/z 103.05 34.27% I ----- I 130 ■ i ' ' ' ' i ' ■ ' ' i 11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #20630: 2-Propanol, 1.1-[(1-methyl-1 .2-ethanediyl)bis(oxy) 59 —4A ' ' I ' ' 11.20 11.40 11.60 11.80 5000 m/z 73.00 30.48%

MJ 31 45 103 ! 39 I 73 : 117 1 ------------- 1 i • ■ ■ ' i ■ • ■ ■ i ' 1 m/z-> 20 30 40 Abundance 50 60 80 70 90 100 #65487: 2-Propanol. 1,1'-oxybis- 110 120 130 A 59 11.20 11.40 11.60 11.80 45 m/z41.0527.59% 31 5000-

89 103 • । 1 11 11' ■ ■ ■ ।1 . .......... 'I 72 I ......................................... ■ ■ i ■ ■ ' । I 1 । । । I । । m/z-> 20 30 40 50 I60 70 80 90 100 110 120 130 11.20 11.40 11.60 11.8

26827.D GCMS1126.M Fri Dec 28 14:53:41 2001 Page 3

NYC-WTC_000032169

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NYC-WTC_000032169Source: NYC Law Department, mirrored locally

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