GCMS analysis comments, sample AD29027, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29027.D Vial: 28 Acq On 11 Dec 2001 3:01 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.46 ug/1 141179 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Propanol, 1,1'-oxybis- 134 C6H14O3 000110-98-5 56 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 _________ 000106-62-7 4 5 Abundance Scan 686 (11.344 min): 29027.D (-) m/z 59.05 100.00% 59

5000

m/z-> 0- 39 II , TP 30 . —44 --++ 40 45

50 60 7080 73

90 100 86 110 103

L 120 130 11.00 m/z 11.20 45.05 M 11.40 11.60 47.51% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxyl 59

5000 45 103 11.00 11.20 11.40 11.60 73 31 m/z 102.95 33.49% -- ............................. ,.......................... 130 • I • 1 1 i I ' • • 1 I ‘ miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087: 2-Propanol, 1,1-oxybis- 59

;j TIT 11.00 11.20 11.40 11.60 31 5000 45 m/ z 73.00 103 _.......... 72 _..... ............ — m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 1Pr l ' 59 11.00 11.20 11.40 11.60 m/ z 41.000 24.51% 5000

m/z-> 31 45 ,,-,.1,----- — - TIP-m 30 40 50 60 73 70 80 90 100 104 110 120 130 130 TTTTpr 11.00 11.20 V/ 11.40 11.60

29027.D GCMS1126.M Wed Dec 12 15:48:29 2001 Page 3

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