Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
NYC-WTC_000017171–000017191Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Chrysene-dl2 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.02 29.50 ug/1 5828990 Perylene-d12 37.11 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 ChWsene-dl2 240 C18D12 001719-03-5 98 2 Naphtho [2,1-b:7,8-b‘]difuran, 1,2,9 240 C16H1602 068873-21-2 50 3 1,4-Bis(6-methylpyridyl-3)-butane 240 C16H20N2 000000-00-0 47 4 <6H-Furo[2 ' ,3 1 :4,5]oxazolo [3,2-a]pyr 240 C10H12N2O5 022423-26-3 43 Abundance Scan 3047 (33.019 mln): 30607.D (-) m/z 240.15 100.00% 24.0
5000
। „ 106 120 1 . ।.... ।.. 42 52 66 78 92 .1 . 132 146156 170180 194 208 222 32.60 32.80 33.00 33.20 33.40 at ll 1. m/z " 24.84% m/z-> 40 60 __ 80 100 120 140 160 180 200 220 240 Abundance #32068: Chrysene-d12 240
5000 32.60 32.80 33.00 33.20 33.40 m/z 239.1 20.05% 106 120 m/z-> ----- 40 60 80 100 120 140 160 180 200 220 111115s... 117121 240 Abundance #32043: Naphtho[2.1-b:7,8-b‘ldifuran. 1.2.9,10-tetrahydro-2 240 32*60 32.80 33.00 33.20 33.40 5000 m/z 241.15 19.27% 211 152 181 197 225 1—I1—B—a————m—m—B—B—m—B——m——nB—mTmBfuo-TDDTTTT mtz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32046:1,4-Bls(6-methylpyridyl-3)-butane 2'0 32.60 32.80 33.00 33.20 33.40 107 m/z 120.05 18.25% 5000 77 120 134 39 51 65 92 —r 1 I ’ ‘ ‘ r* rr r-p miz—> 40 60 80 100 120 140 160 180 200 220 240 32.60 32.80 33.00 33.20 33.40
30607.D GCMS0103.M Thu Jan 10 14:56:32 2002 Page 12
NYC-WTC_000017189
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NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017299
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder