Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 1,1,1,5,7,7,7 -Heptamethyl-3,3- Concentration Rank 1
R,T. EstConc Area Relative to ISTD R.T.
17.45 5.59 ug/1 3305740 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethy1-3, 3-bis (t 444 C13H40O5Si6 038147-00-1 27 2 2H-1,4-BenzodZazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 4 Pregnane- 20-dione, 11-[(trimethyl 462C26H46N2O3Si 057305-27-8 9 Abundance Scan 1351 (17.447 min): 30709.D (-) m/z 73.00 100.00% 73
5000 341 ......... M........... 147
m/z-> mH 45 , 97 117 [ 179 207225 251 281 311. ( A m/z 341.00 SS1 397 TICIIUCCOgT . .p .V, p'n. p.. rprt. pl I! p p ri. IA,. p,.. p... p ,.. I 40 60 80 100120140160180200220240260280300320340360380400420 429 17.20 17.40 17.60 17.80 28.40% Abundance #56714: 1,1,1,5,7,7,7-Heptamethy-3,3-bis(trimethylsiloxy)t 73
147 5000 267 355 429 17.20 17.40 17.60 17.80 45 207 m/z 147.00 14.36% -I ■ >. l. ■,. > l ■ > I r 111111 ■ I ri 11 l l I—000—010——10—0010317" ' ri p 11111 11111111 hmmpp m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337: 2H-1 4-Benzodiazepin-2-one, 7-chioro-1 3-al hydro-5- 73 341
17.20 17.40 17.60 17.80 5000 m/z 342.00 9.50% 45 91 | 116 146 227 269 315 | m/z-> 40 60 80 100120140160180200220240260280300320340360380400420__ ...................... Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 73 17.20 17.40 17.60 17.80 m/z 325.00 9.27% 239 5000 342
45 | 133, 179 211 ....................... ....................... TPTTTn 101100010—000101011 314—11010—t0070—00—1—101133001117 m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 17.20 17.40 17.60 17.80
30709.D GCMS1126.M Mon Jan 28 11:32:48 2002 Page 3
NYC-WTC_000004312
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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