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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004313
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 2-Propanone, 1-(1-methylethoxy Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

18.15 0.45 ug/1 287524 Acenaphthene -dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone /I-(1-methylethoxy)- 116 C6H1202 042781-12-4 17 2 2-Propenenitrile, 3-(acetyl oxy)- 111 C5H5NO2 014268-54-3 16 3 Acetone 58 C3H60 000067-64-1 9 4 2-Butan , 2-nitroso-, acetate (est 145 C6H11NO3_________ 013880-90-5 9 Abundance 1......... " Scan 1428 (18.154 min): 30709.D (-) m/z 43.05 100.00% 43 57 73 5000 111 95 17.80 18.00 18.20 18.40 ' m/z-> m T rpm , 85 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 , 127 146 201 TDTNPWTTNPag m/z 57.00 69.32% Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43

5000 17.80 18.00 18.20 18.40 27 m/ z 73.00 56.77% 11, ill,1 ....58;.....73................................. ........... ....... ■" r " ■ i"1 ■ i ■ ■ 1111 ■ ■ (11,11'"«।1'111 ■11 * t1 *" i1 * ■ ‘ i “ " i • ■k 111"' ("1' i1" *r7 " r "' r " ■ r11 ’I"111 m/z-> 10_20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance 2407 z-Fmpencrititle. 3-(acetyloxy- 43 111 — , । .t m . i , j r i TI 17.80 18.00 18.20 18.40 5000 m/z 111.10 45.26% 15 77 ..... ;............. 52........... !....... 94....... |,..................................................... 1 1" ‘ r1 ■ ■ i ■" ‘ i" " i1'" i ■'1 ■ i ■ ■" i" " i ■" ■ r ■ ■ ■ i'"' i1 ■" r ■ “ i" " i •"11" " in ITI'11111'1111''11''111 m/z->_____ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #94: Acetone 5 ..................... . T I-1 43 17.80 18.00 18.20 18.40 m/z 69.10 28.76% 5000 15 58

T r "' i ■"1 r ■" r "' i" " r1" i" " 111" 11111 ’T77111111111111'1' I'1'' 111'11 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140 150 160170 180 190200 17.80 18.00 18.20 18.40

30709.D GCMS1126.M Mon Jan 28 11:32:53 2002 Page 4

NYC-WTC_000004313

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NYC-WTC_000004313Source: NYC Law Department, mirrored locally

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