GCMS analysis report for sample AE01231, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1802\1231.D Vial: 38 Acq On : 18 Feb 2002 2:10 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

20.92 0.24 ug/1 21206 Acenaphthene-dl0 21.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,l,y, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxane, 1,1/1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 40 3 Propanedioic acid, [(trimethylsilyl 336 C12H2805Si3 038165-93-4 23 4 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 73.00 100.00% 17 Abundance.......... ’....................... " Scan 1730 (20.922 min)f 1231.D()................................... ............... m/z 73

5000 147 281 ................. .........A. 327 20.60 20.80 21.00 21.20 45 1 '-| * r 221 t i,. 4M5 m/z 147.10 39.94% m/z-?... 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 ...... ./0 20.60 20.80 21.00 21.20 221 281 327 m/z 281.00 37.68% 415 519 561 i ’ I’’ miz—? 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 147 281 20.60 20.80 21.00 21.20 5000 m/z 326.90 15.01% 369 207 338 249 m/z->_____ 50___ 100__ 150__ 200 __ 250......300 350 __ 400 450 500 __ 550 Abundance #73507: Propanedioic acid, I(trimethylsilyl)oxy]-, bis (trim ■ ' i ■ ■ ‘ ‘ i ‘ ' i ' 1 1 ' I ■ 1 ■ ' i 73 20.60 20.80 21.00 21.20 m/z 282.00 11.12% 5000 147 45 102 --—L 177 221 I ' ‘ ' ' I ' ' ‘ ■ i ‘ 292 321 ' ‘ i ' ' ■ ' i ‘ ‘ ' i ' ' ' ' i ■ ' ' ■ i ' ' , ... H, ,, m/z-> 50 100 150 200 250 300 350 400 450 500 550 20.60 20.80 21.00 21.20

1231.D GCMS0208.M Thu Feb 21 09:33:18 2002 Page 4

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