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GCMS analysis results for sample AD31380, Feb 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31380 conducted on February 7, 2002.

NYC-WTC_000016213–000016222

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31380.D Vial: 11 Acq On : 15 Jan 2002 8:44 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethylene oxide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

34.92 0.64 ug/1 58261 Perylene-dl2 36.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethylene xide 44 C2H40 000075-21-8 3 2 Acetalde yde 44 C2H40 000075-07-0 3 3 Propan 44 C3H8 000074-98-6 1 4 Urea, utyl- 116 C5H12N20___ _ 000592-31-4 1 Abundance Scan 3255 (34.923 min): 31380.D (-) m/z 39.95 100.00% 43

5000

34.60 34.80 35.00 35.20 64 78 96 49—nnnnmImmmmdLTO/m ddn 207 1 1 i ■ ■ m/z 43.95 46.68 m/z-> 20 40___ 60___ 80 100 120 140 160 180 200__ Abundance #62267: Ethylene oxide 29 44 15 5000- 34.60 34.80 35.00 35.20 m/z 44.85 0.83 । I 1,"a ■ I11' m/z->___ 2Q AQ 60 80 100 120 140 160 180__ 200_ Abundance /30: Acetaj jonv 29 44 34.60 34.80 35.00 35.20 5000 m/ z 35.90 0.76

m/z-> Abundance ' ‘2b' 29 40 60 80 100 120 140 160 #62269: Propane 180 200 ArwAh.AaMYWmaAAAM 34.60 34.80 35.00 35.20 ‘ m/ z 45.95 0.49 5000 44 15 .1 1 TTT ■ 1 i ■ ■ ‘ ■ i ■ ■ ■ 1 1 ■ ■ ■ ■ i ‘ ■ 1 ■ ■ • ■ 1 ■ 1 1 ■ 1 ■ r ' ' 1 ' 11 r1 r miz-> 20 40 60 80 100 120 140 160 180 200 34.60 34.80 35.00 35.20

31380.D GCMS1126.M Mon Feb 04 15:09:54 2002 Page 2

NYC-WTC_000016221

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