GCMS analysis report for sample AE01221, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1502\1221.D Vial: 35 Acq On : 17 Feb 2002 2:20 am Operator! 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.34 ug/1 28417 1,4-Dichiorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane,/2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 3 2-Methyl-5-hexen-3-ol 114 C7H14O 032815-70-6 9 4 3,4-Dimethyl -5-hexen-3-ol 128 C8H160 000000-00-0 9 Abundance Scan 345 (8.213 min): 1221.D (-) m/ z 73.00'166.00% 73

5000 43 ------ 87 103 7.80 8.00 8.20 8.40 8.60 ++ 51 57 htmm i “ ■11 “ “ i' “' i 1—— m/ z 43.05 43.72% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63526: Butane, 2-methoxy-2-methyl- 73

5000 i ■ ' ' ■ i ■ • 55 7.80 8.00 8.20 8.40 8.60 87 m/ z 45.0,5 15.35% 27 45 I 33 '' I ‘1111 ‘11' 1111' I ‘ ! i11 • • i1' * * i» 1’I0O00———0’002-3 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance 53673 -Pentanci, zme 73

7.80 8.00 8.20 8.40 8.60 5000 m/z 41.0,5 14.98% 55 45 87 27 39 m/z-> 2D 25 30 35 40 45 50 ^ 60 65 70 75 80 85 90 95 100 105^110 Abundance #3017:2-Methyl-5-hexen-3-ol 73 7.80 8.00 8 20 8.40 8.60 55 m/z 71.0,0 8.01% 43 5000

27 mm Imph ilin....... hi 1 I 1 1 ‘ ‘ I ' 1 1 1 I ‘ 1 1 1 I' ' 11 I ■' r m/z~>____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 7.80 8.00 8.20 8.40 8.60

1221.D GCMS0208.M Thu Feb 21 09:28:22 2002 Page 1

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