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GCMS analysis results for sample AE02973, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02973 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005689–000005697

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\FEB0802\2973.D Vial: 37 Acq On 9 Feb 2002 8:17 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7FB Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.22 2.66 ug/1 351946 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-me thoxy - 2 - me t hy l - 102 C6H140 000994-05-8 36 2 3-Pentanol 3-methyl- 102 C6H140 000077-74-7 28 3 1,3 -Dioxol ane, 2-methyl- 88 C4H802 000497-26-7 9 4 Silane/ tetramethyl- 88C4H12Si 000075-76-3 9 Abundance / Scan 346 (8.222 min): 2973.D (-) | m/z 73.00 100.00% 73

5000 43 / 7.80 8.00__ 8.20 8.40 8-60 m/z-> +38,1450 55+59— 67+4 4 87 103 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 TTTTTTITTTTTTTTHWTTTITT m/z 43.05 37.09% Abundance #1761: Butane, 2-methoxy-2-methyl- 73

5000- . 2....... 7.80 8.00 8.20 8.40 8.60 55 87 m/z 45.0.5 13.68% 45 .. 27 33 TItvungrutrjui " I " " I'1" I "11111" I" " i" TTI I ■ ’" r ‘ " i ■ ■' • r ■ m/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance ' . 73 l ■ ■ ■ > i ■ ■ 7.80 8.00 8.20 8.40 8.60 5000- m/ z 41.05 12.29% 55 45 87 27 rTTTTTTTTTTTTpnT-rpnT-rp-rrTpTTTyrTTTpTTT-pTT-qTTTTp^TTp-rrTT^^ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62902: 1,3-Dioxolane, 2-methyl-.............. . .....-.... ...... 73 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.83% 5000 43

58 27 87 0 ...... I ’ I " I 1....... . I l H I .... | T7 r r | .! I ! | I I 1 I | 1 I 1 I | I I I I | I | I ! | | | | | | , I | I | | | , I | I I ! I | M H | I 1 ! | | , , m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 7.80 8.00 8.20 8.40 8.60

2973.D GCMS0208.M Wed Feb 13 11:12:55 2002 Page 1

NYC-WTC_000005696

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NYC-WTC_000005696Source: NYC Law Department, mirrored locally

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