GC/MS calibration data for sample 28323, Dec 2001

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Data File : C:\HPCHEM\ 1\DATA\DEC2 701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 * MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

7.62 1.95 ug/1 742137 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2 -methoxy- 2-methyl- 102 C6H140 000994-05-8 36 2 3-Pentanol, /3-methyl- 102 C6H140 000077-74-7 36 3 1,3 -Dioxolane, 2 - (1 -methylethyl) - 116 C6H1202 000822-83-3 25 4 2-Methy1-5-hexen-3-ol 114 C7H140 032815-70-6 23 Abundance - d - Scan 280 (7.618 min): 28323.D (-) m/z 73.0.0 100.00% 73

5000 43 I ‘ ‘ 1 ‘ I ’ ‘ ‘ ’ I ‘ ‘ ‘ ‘ I ‘ ■ ■ i ■ ■

87 103 7.20 7.40 7.60 7.80 8.00 . ............ . +r 126 • i • ■ ■ ■ i ■ ■ > i I * i m/ z 43.00 3 8.04% m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1761: Butane, 2-methoxy-2-methyl- 73

5000 A —KmTpTTTTTT 7.20 7.40 7.60 7.80 8.00 55 87 m/z 41.00 13.29% 45 27 33 1 1 i1[iir jii11।iiri]11iijiiii[ir I ■ i ■ • • '4 ••••!■ ■ i■ 4' ■ i■ ■ ■ • i ‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63573:3-Pentanoi, 3-mcthyi ; 73 J —----- i ■ ■ ' 1 i 1 ■ i ' ■ • ■ i ■ ■ ■ ■ i ' ■ 7.20 7.40 7.60 7.80 8.00 5000 m/z 45.05 12.88% 55 27 45 87 39 ■ i ■ • • ■ i • ■ ■ ■ i • ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ' 1 ' ■ i ■ ■ ■ ■ i ‘ ■ i ‘ ■ 1 ' i ■ ‘ ■ i ■ ■ ■ ‘ i ■ ■ mtz~> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64281: 1,3-Dioxolane, 2-(1-methylethyl)- 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 7.89% 5000

27 39 45 56 1 ,1 ■ ■ i ■ ■ 86 115 ■ I 1 ‘ ■ 1 1 ‘ 1 ' i • 1 ■ ■ i ■ • ■ ■ i ■ ■ ■ • i • • ■ ■ i ' ■ —FPPt1—TTPr miz-> 20 30 40 50 60 70 80 90 100 110 120 130 7.20 7.40 7.60 7.80 8.00

28323.D GCMS1126.M Wed Feb 06 13:01:22 2002 Page 1

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