GCMS calibration table for sample AE09449, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0202\9449.D vial: 8 Acq On 2 May 2002 9:39 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C : \DATABASE\NBS7 5K. L

Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 8.09 0.64 ug/1 56296 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, /2 -methoxy-2-methyl - 102 C6H140 000994-05-8 36 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 3 N-Ethy formamide 73 C3H7NO 000627-45-2 9 4 Pentape, 3-methoxy- 102 C6H140 036839-67-5 9 Abundance 7 Scan 333 (8.089 min): 9449. D (-) m/z 73.10 100.00% 73

5000- 43

7.80 8.00 8.20 8.40 1 1 1 1 1 ■ 1 i ' ' 1 1 i 1 | 149 55. — 111 1 I ■ ' ' ' | T-r 1 'i' , 1 1, I J ] I I 87 103 l l | i ■ I I | I 1 I ! ! | I m/z 43.05 33.51% m/z-> __ 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- 73

5000 1 U ' i ' 1 ' 1 1 1 1 । 1 i 1 ■ T’I 1 1 1 1 7.80 8.00 8.20 8.40 55 87 m/z 45.05 11.58% 2 45 27 33 | TTIm ——————— m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73 A m/z 7.80 8.00 41.05 Y — 8.20 8.40 11.41% 5000 55 45 87 27 I ( 39, r, ■ । ■''' । ....................... ,I...................... m/z-> 10 20 30 40 50 60 70- 80 90 100 110 Abundance #292: N-Ethylformamide nAmipp)............ 33 7.80 8.00 8.20 8.40 73 m/z 71.10 7.72% 5000 44 58

15 1001 — +,11—, — | । I ' 11 i । । T I-1 ll ] I । i ' | ' I I I i | i

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

9449.D GCMS0501.M Fri May 03 08:41:20 2002 Page 1

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