GCMS calibration table for sample AE09449, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\MAY02 02 \ 944 9 . D Vial: 8 Acq On 2 May 2002 9:39 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 8.32 ug/1 728595 1,4-Dichlorobenzene-d4 12.19 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CHCJ12C (O) OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 5 Abundance Scan 341 (8.163 min): 9449.D (-) m/z 43.05 100.00% 43

5000 59 l I |—I I I I ['ll T “I | I ! I I | I I I I | I 101

m/z-> 10 20 30 38 I 40 ,1 ,i 53 50 , , 67 * 1 ' 1 1 1+‘‘‘I 60 183 rll 70 80 90 + 100 110 m/z 7 80 8.00 59.10 8.20 8.40 42.45% 8.60

Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 ~1 ' i ' ' ' ' I ' 1

m/ z 780 8.00 58.10 11

8.20 L | I I ii

8.40 |

16.65% i r l

8.60 | k

27 101

m/z--> - — .................... । 10 20 30 40 +4950— 60 IIIII111’ 70 80 83 90 1 i 1 1 1 ' i ' 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 l i | i i i । | । i 11 | i i i T | i I i r-[ t-

7 80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.53%

7 I [ ! I T I 'I | I I I I | 72 I I ' i 1 1 1 1 i 1 ’ 1 1 1 1 ' 1 1 i 1 100 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 6.93%

5000 15 58 27 T 1 1 | i'll I | I ,11, I I I i ' । 1 I | I | | | | l I I | I | I I [ ! ! I 1 > I I I | I ' I ' ' ii । i i । I । । । Ki । m ! । । i fi । । 11

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9449.D GCMS0501.M Fri May 03 08:41:21 2002 Page 2

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