GCMS analysis report for sample AE09524, May 2002

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Data File C:\HPCHEM\l\DATA\MAY0202\9524.D vial: 22 Acq On 3 May 2002 11:38 am Operator: Sample GC/MS SCAN 4/22 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.16 15.03 ug/1 824425 1,4-Dichlorobenzene-d4 12.20 Hit# of 5/ Tentative ID MW MolForm CAS# Qual

1 2 - Pentanone, 4-hydroxy-4-methyl - 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C (0) OCH3 100 C5H802 003724-55-8 9 3 5-Hexen-2 -one 98 C6H10O 000109-49-9 7 4 Acetone 58 C3H60 000067-64-1 7 Abundance Scan 341 (8.165 min): 9524.D (-) m/z 43.00 100.00% 43

5000 59 ................... 1 1 m i k _ i i i 1d i i । i- 101 780 8.00 8.20 8.40 8.60 .................................. 38 । 53 , 69I I I I I I 83 | I I-—1 I I | I I l~T ] I I I I j I ti ' ‘ I I-1 1t I ‘ I I I I I I I I '] t I I —I I m/ Z 59.10 42.36% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 1 I I I I I I I I I I “I I 1 I I I I I-

59 780 8.00 8.20 8.40 8.60 m/ Z 58.10 16.29%| 27 101 ............. ■ +49 83 ■ 1 । 1 1 11 । I ' 1 1 1 i ■ 1 ■ ■ i ''' 1 1 i f । ■ ■ ■ ■ । ■ m/z-> 10 20 30 40 50 60 70 80 ' 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 __________ ____ _ । r _____ 11 | i l i [ i iii । m " ।—।—।—] i it

7.80 8.00 8.20 8.40 8.60 5000 m/ z 101.15 12.90%

58 i ■ ■ ■ 1 i ' 1 1 1 i 384 I———— 1 72 100 10* m/z—>. 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one 43 7.80 8.00 8.20 8.40 8.60 m/ Z 41.05 6.62% 5000-

55 ........ 15 1 .........27 1......... 38 50 | 83 98 Irmfrss 7 I-1 I I I i | I I I I | I I I I t 7 ‘ ] i ii I [ I I I | | | | | —J 1 | | | | | |—|—[—1—|—|—|—|—| । । । "14 °0 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9524 .D GCMS0501 .M Fri May 03 12:28:33 2002 Page 1

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