GCMS calibration table for sample AE09449, May 2002

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Technical document displaying GCMS calibration data and compound retention times for sample AE09449 processed in early May 2002.

NYC-WTC_000045507–000045515

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0202\9449.D Vial: 8 Acq On 2 May 2002 9:39 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Anthracene-d10 - Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.72 0.46 ug/1 53404 Phenanthrene-dl0 25.58 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

I Anthracene d10-( ' 001719-06-8 87 188 C14D10 2 Phenanthrene-d10 001517-22-2 87 188 C14D10 3 4-Methyl-2- (3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 42 4 Pentacyc/o[8.4.0.0(3,7) .0 (4,14) .0(6 188 C14H20 000000-00-0 36 Abundance 7 Scan 2257 (25.720 min): 9449.D (-) m/z 188.15 100.00% 188

5000

80 94 i i । 1 I T i । i iTi । i i < i । i i i i |

43 52 66 Till 156 25.40 25.60 25.80 26.00

m/z-> ( | I I I । | I I | 1 | I i r i | i I I i [ it 117 I

1 । [ I I L • । T i | I I I I [ I i—i—i—r 5000 25.40 25.60 25.80 26.00 m/ z 80.10 17.15% 80 94 160 I I > I I I I I I I I I m 66 jl I I I I I I I । । > । । । । । । > । । > । > । । । । ■ । । > । । । । । I I | । । i i । । । i । । rl‘I r " ■ i m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 ... .............. Tn । । । । । | । । । । n r~i [1 ‘"I i T 25.40 25.60 25.80 26.00 5000- m/z 189.15 13.02%

80 94 160 1 66 m—WIWTITTTTOTTTT - . rrl 111 ■ । BBII/0 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1 1 | 1 I L y — I I I I I I I I 1 I I—I" Abundance #19859:4-Methyl-2-(3-fluorophenyl)pyrimidine 188 25.40 25.60 25.80 26.00 m/z 184.15 11.68% 5000- 121

67 173 94 ■ । ■ ■ ■ ■ । ■ ■ - ■ । ■ 1 75 _....... 146 161 ...... I I ' I I I I I I r I I I I I I I I I I I I I I I I I I I I I | I । । । | II I) | I I I I | I ! I I | I I I I | I I ! I | | ! I TTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9449.D GCMS0501.M Fri May 03 08:41:22 2002 Page 3

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GCMS calibration table for sample AE09447, May 2002 · Box DEP Box 25

NYC-WTC_000045472

Technical document displaying GCMS calibration data and compound retention times for sample AE09447 processed in early May 2002.

1 shared topics · Same agency, volume and box · similarity 0.997