GCMS calibration table for sample AE09391, May 2002

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Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.

NYC-WTC_000045452–000045461

Folder label: “GCMS X 5/3/02 A 5/8/02”

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Data File C:\HPCHEM\1\DATA\MAY0102\9391.D Vial: 10 Acq On 1 May 2002 4:20 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L

Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 25.72 0.45 ug/1 37257 Phenanthrene-dl 0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -d10- 188 C14D10 001719-06-8 2 Phenanthrene-d10 188 C14D10 001517-22-2 3 -(4-Tolyl/-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 4H-Pyrido[1,2-a] pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 28 Abundance Scan 2257 (25.719 min): 9391 .D (-) m/z 188.15 100.00% 188

5000

80 94 1 L I I I I I I I I I I I I I I I > I I I I

44 = 66 160 I I 25.40 25.60 25.80 26.00

m/z-> — 36+44 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 r 1111 i111' i । ■ 111 ■ ■ ■ > । ■ ■ ■ ■ । ■!" ■' m/z 94.10 19.77% Abundancei #19957: Anthracene-d10- 188

5000 ---------- 25.40 25.60 25.80 26.00 m/z 189.15 18.00% — 80 94 160 66 1 I | I I I > | I I I . | I I I I | I I I ! | I ! I I I > I I >1 | I I I I f I I I I I I I I I I I I I I I I I I I I II I[ II I I I I I ...... hl 1... " ।■11 t’ltrorrr m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 1 ' | 1 1 ' 1 | I I T, |-T I-l -I '| ! I I I |

25.40 25.60 25.80 26.00 5000 m/z 80.00 17.98% A 80 94 160 66 11 ■ 111 ■ 11 > । ■ 114.

m/z-> 30 ■ i ■ • ■ > । ■ ■ ■ ■ i ■ ■ ■ ■ ।

40 50 60 70 ■ I ■ । ■ H i " 1 1 r ' " i 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one ) 111 188 25.40 25.60 25.80 26.00 91 m/z 44.05 14.62% wANwWpw 105 5000 119 .. .......................... .65 _ 1. | 146 i । I । 1 i । । Il । । । । i । । । । । i । । P । r। <111 ■ ■ • ■ । ■ ■ > ■ । ■ ■ ■ ■ । ■ IIT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9391.D GCMS0501.M Wed May 08 14:14:35 2002 Page 4

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