GCMS calibration results for sample AE09334, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR2502\9334.D Vial: 11 Acq On : 25 Apr 2002 10:26 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.72 0.23 ug/1 58008 Phenanthrene-dl0 25.59

Hit# of 5 entative ID MW MolForm CAS# Qual

l Anthracene/diO- //7 188 C14D10 001719-06-8 42 2 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 40 3 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 40 4 Phenanthrene-d10 188 C14D10 001517-22-2 38 Abundance 7 Scan 2252 (25.722 min): 9334. D(-) m/z 188.10 100.00% 188

5000

"I I I I I I / 11 I I I I I __________ II I I I I I l [ I 94 25.40 25.60 25.80 26.00 42 66 80 ........ 132........ 158........ | L m/z-> । i i i pl 1 t rper i 1 । i I I i [ rrl I j' r 40 50 60 70 80 -H i ■'111'11111 ‘■ r 11 ■ i''111' ■r • i111' i111 90 100 110 120 130 140 150 160 170 180 190 m/z 184.10 15.67% Abundance #19957: Anthracene-d10- 188

1 5000 17 25.40 25.60 25.80 26.00 m/z 94.05 12.52% 66 80 9|4 IfO i>j।i।r n11|1H n n n|>>।<।II<n .>i।।।i।।।।!।।।।।!!।in- n | r ....... .. ......... m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- 188 173 1‘14/‘11/T1I**I"*I 145 25.40 25.60 25.80 26.00 5000 m/z 189.05 10.59% 102 A 114 130 76 94 TTPTTTTTTTTHI- 157 -P III । i ] । i ii । । n । । ।' ITT L m/z--> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one ' 1 1 1 1 ' ' I T 1 ' 1 I 1 1 ' '■ I । । ' । I 188 25.40 25.60 25.80 26.00 91 m/z 79.95 10.55% 105 5000

119 65 _ ..... ...... 1..... 1111'111 146................ |I.... I I I I I I I I I I I I j I "I I I I II I I I I I I I I I I I I I I I I I I I I I I r I I I I I J TIl m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9334.D GCMS0412.M Fri Apr 26 08:19:13 2002 Page 3

NYC-WTC_000046358