GCMS calibration results for sample AE09334, April 2002

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Laboratory report showing GCMS calibration data for sample AE09334 generated on April 25-26, 2002.

NYC-WTC_000046351–000046359

Folder label: “GCMS X 5/7/02 A 5/9/02”

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Data File : C:\HPCHEM\l\DATA\APR2502\9334.D Vial: 11 Acq On : 25 Apr 2002 10:26 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Acetylthiazole Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 8.25 0.66 ug/1 117468 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Acetyl thiazole 127 C5H5NOS 024295-03-2 12 2 1-Octadecanol 270 C18H380 000112-92-5 10 3 N-Acet/lpyrrolidone 127 C6H9NO2 000932-17-2 10 4 Nonadecanol 284 C19H40O 052783-43-4 9 Abundance Scan 349 (8.252 min): 9334.D (-) m/z 43.05 100.00% 43

5000 125 । i “i " i" । m l | i r r । p i r i I ] ri "I 1 . 63 82 97 8.00 8.20 8.40 8.60 | , , , I'1,11!! l',, fL ,, th, , I , 11 i Ii i IfbII r j i i i ‘ITl ........................................................ "tqvutT । II 661 i I 7 111 m/z 124.85 20.39% m/z-> 20 40» 60 80 100 120 140 160 180 200 220 240 260 Abundance #4717: 2-Acetylthiazole 43

5000- "s’."* I I I I 1 1 I 1 ' 1 1 i 1 1 ' 99 127 8.00 8.20 8.40 8.60 58 112 m/ Z 46.95 13.29% | r ' i 1 1 1 'i ■ 1 1i ' 1 ' i 1 r1 1 i 1 1 1 1 I ' 1 ■ ' I 1 ' ‘ ■ i ‘ ■ ■ ■ i 1 1 ' ' i 1 1 ' 1 i 1 1 m/z-> 20 40 60 100 120 140 160 180 200 220 240 260 Abundance #72027:1-Octadecanol 43 IF"/1 8.00 8.20 8.40 8.60 5000 82 m/z 96.95 13.16% 56 68 | 97 111 ‘ 1 1 1 1 1 r‘1 1 r' 11125.......... 224 .... 270 । । i i I r r । 1 । i i ।'। । i i i-1 । । । । i । । । । ! ।11 । । । । । । 1 l i — m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #4732: N-Acetylpyrrolidone I 43 8.00 8.20 8.40 8.60 m/z 126.90 12.72% 5000- 99 127 56 86 301 1 1 1 1 i ■ 69 | | , 112 1 ' । 1 ■ ' ' i ■ 1 ■ ‘ i 1 1 1 1 i 1 1 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 8.00 8.20 8.40 8.60

9334.D GCMS0412.M Fri Apr 26 08:19:12 2002 Page 2

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