Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
NYC-WTC_000036220–000036231Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\DEC1001\29291.D Vial: 11 Acq On : 12 Dec 2001 9:29 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propen-l-ol, 2-chloro-, acet Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
7.74 0.56 ug/1 144708 1,4-Dichlorobenzene-d4 11.67
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propen-l-ol, 2-chloro-, acetate 134 C5H7C1O2 000692-72-8 9 2 2-Hexen-l-ol, acetate, (Z)- 142 C8H14O2 056922-75-9 9 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 4 4 Glycine, N-acetyl- 117 C4H7NO3 000543-24-8 4 Abundance Scan 294 (7.741 min): 29291 .D (-) m/z 4 .95 100.00% 43
5000- • 1 i • 1t '| । i i > । m । । । i i । । 35 97 125 7.40 7.60 7.80 8.00 49 61 75 82 Tr 11 ——nnat r ■ I +T • i1 ■ • 11• ।»• t • •117 |, • p . >. p . 11 ( - • • । m/z 124.85 12.71% miz-? 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6026: 2-Propen-1-ol, 2-chloro-, acetate 43
5000 99 T T 7.40 7.60 7.80 8.00 57 m/z 96.85 9.63% 75 92 —37 + , 49 ■ ''i1 । । . TP I ‘ ' i ■ • ‘ 1 i • • ■ ■ i ■ 1 ■ 1 i ‘ ‘ ■ i miz- 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance -66153: 2-Hexen-1-ol, acetate. (Z)- 43 ' ■ i ‘ ' i ■ ‘ 1 i 1 1 “ ' i ' 1 1 • i 7.40 7.60 7.80 8.00 5000 m/z 35.00 8.13% 67 57 82 73 100 142 111188 .-n-r-p- .-r-rp-T-r ■ • J t i >’s ? r t H —II 1TTIT • ! ‘ ‘ l miz- 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #4732: N-Acetylpyrrolidone 43 7.40 7.60 7.80 8.00 m/z 98.95 6.67% 5000 99 127 30 [ 56 69 , 112 —mmp ■ > t * • T-p-r-T-rp- • ‘ • rp i > > p . ■. p > > i p > >. p ।. ■ i ‘ I ‘ ‘ ' I ‘ ‘ < I ‘ 1 1 ' P 1 ■ ‘ I miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 7.40 7.60 7.80 8.00
29291.D GCMS1126.M Wed Dec 19 12:54:25 2001 Page 2
NYC-WTC_000036228
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NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder