Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
NYC-WTC_000036220–000036231Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC1001\29291.D Vial: 11 Acq On : 12 Dec 2001 9:29 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
11.34 1.18 ug/1 306861 1,4-Dichlorobenzene-d4 11.67
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3 ,30 - oxybi S- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1, 11 -oxybis- 134 C6H14O3 000110-98-5 50 4 2-Propanol,/ (1- (2-methoxypropoxy) - 148 C7H1603 013429-07-7 50
A Abundance "" ........ 7 Scan 686 (11.340 min): 29291 .D (-) m/z 59.05 100.00% 59 1
5000 45 73 103 • ■ i ■ • ‘ I ‘ * 1 * I 1 1 TIt I I I I J
—l
N 11.00 11.20 11.40 11.60 85 — i * i TTBemTgr I ‘ ‘ ‘ ' I ‘T1 l | 1 1 1 1 | I m/z 45.05, 47.79% miz-? 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59
5000 T ! ; . . —51111 r-r-T-T T TT . . I 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05. 35.03% TTI I Ji i । ■ । । — 1 > PIp । Jl i __________ 130 i । TTI TTm—ni TT—ng) ■ i ■ ■ •' i • miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3.3-oxybs- i 59
11.00 11.20 11.40 11.60 •
AA 5000 31 45 m/z 73.00 29.08% 103
1 T j | I l’| 10—1,————— j • । । TIWTTITT 1 I p l TTI < I I TIIITnr 134 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087:2-Propanol, 1,1‘-oxybls- TIIT 7-1-q-rr T T ' ,-r-r-T-i j i r i r-j- 59 11.00 11.20 11.40 11.60 !
A m/z 41.05 23.78% 31 5000 45 103 89 ‘ i ■ ■ ■ ‘ i • ■ ' ■ i ' * • i72 1 ■ • ■ i 1 1 1 1 I 1 1' 1 I Tr ’In60118 . . . । > i . > |-r TI -.-r-r-r-, r-n-r-j- miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60
29291.D GCMS1126.M Wed Dec 19 12:54:29 2001 Page 3
NYC-WTC_000036229
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NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder