GCMS sample analysis report AE05844, Apr 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR1202\5844.D Vial: 20 Acq On 16 Apr 2002 2:42 am Operator: Sample re-extract Inst : 209 Mise Multiplr: .1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.75 0.22 ug/1 41150 Phenanthrene-dl0 25.61 Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------- 1 Anthracene-d10- 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 50 3 5-Methyl-2/phenyl-2-hexenal 188 C13H160 021834-92-4 9 4 Pentacyclc/[8.4.0.0 (3,7) . 0 (4,14) . 0 (6 188 C14H20 000000-00-0 9 Abundance 7 Scan 2256 (25.753 min): 5844.D (-) m/ z 188.10 100.00% 188

5000 ........../................... ' 1 ' ' ' ' I | I I I ! | I I 78 25.40 25.60 25.80 26.00 44 54 " " i ■ ‘'1111'' i " 111''1 66 , . y........... i6°.. i i i । [ I I । i । । । । i । । । > । । । । । । I r । । । । । । । । । । । I I J i r r r ITI’ m/z 189.05 21.61% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 - ‘TT 25.40 25.60 25.80 26.00 m/Z 184.00 14.15%

| 1 । | | t । । । 66 80 94 160 ||| । । । I > । > > > < | > > । । । I I । । । । i i | | i I | i | i | i | | n i'i-| i rr i । i > I I | i i i i । i । i । । iTr । i i

n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 .......... /............................ tIB" TT । ,TiT ।' i i I I | । i : i | i 25.40 25.60 25.80 26.00 5000 m/z77.95 12.77%

80 94 160 66 ■ । ■ ■ ■ > । ■ > ■ ■ । ■ • ■ • । > ■ ■ •! ■ ■ 111 ■... । . n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69187: 5-Methyl-2-phenyl-2-hexenal ........ — ' I ‘ 1 ' ' I ...................... n p । । । । t IT ‘I’ 188 25.40 25.60 25.80 26.00 rn/z 80.00 12.25% 117

5000 104 132 145 173 .................... | .. I.. " i ' 1 1 1 i ■ ■ r 1 1 1 i ‘ 1 1 1 1 1 1 1 1 I 1 1 1 1 1 1 1 111111111 -H— ’ I' ‘' I " " 111 II’ ........../.................................. ' i 1 1 1 ' i 1 T' 1 i 1 1 1 1 1 1 1 1 ' 1 1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

5844.D GCMS0412.M Wed Apr 17 09:47:17 2002 Page 3 NYC-WTC_000048521