GCMS results for unknowns, sample AD31130, Feb 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0902\31130A.D Vial: 27 Acq On : 10 Jan 2002 4:30 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

14.17 0.24 ug/1 84491 Naphthalene-d8 15.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 45 2 Benzoic acid, 2,/5-bis (trimethyl silo 370 C16H30O4Si3 003618-20-0 43 3 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 4 Benzeneacet 16 ac id, .a lpha 4-bis [ ( 326 Cl 5H2604Si2 055334-40-2 37 Abundance Scan 994 (14.167 min): 31130A.D (-) m/z 73.0,0 100.00% 73

5000 267 355 .......... H............ 45 , i, 154 177 193 223 251 13.80 14.00 14.20 14.40 I, T r r A । t' j ■: t । t 1 t 1 j f 133 323 339 । i fipu t ’ i 1” । 1M t iti 1 M 1 i 1* 1 1 rj i Prryr —l—---’**)o*****m2*8d*m ’ ‘I“ m/z 266.99 32.35% m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

5000 267 355 ....... A........ 13.80 14.00 14.20 14.40 m/z 355.0 22.98% 191207 251 323339 ’0019000000090*" ——— j' * > * i miz->_ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance $73578 Sonzulc acid 2.5-bistnmetryslicxy)- thiethvis • 73 355 1 । • ■ ■ ■ >1 • ■ • r • ■ ■ ■ । ■ ■ ■ ■ । • 13.80 14.00 14.20 14.40 5000 m/z 267.90 9.32% 45 , 147 179 207223 , 267282297 370 TTTT ’I1’119999B31mB11T9mRT_TTTTOIIITI i •11 ■ 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methyIene] 1 i • 1 • 1 r1 Mis [ । । । । । । । i i । । 73 13.80 14.00 14.20 14.40 m/z 74.00 8.01% 5000 267 44 | 151 179194209 250 ‘' i1 “ 111 ‘‘‘4141444*1—44*192241*4/7448414***2*8**148**14 ‘' 11" ‘ i “ “ i “ “ I" " I •'' ‘ I ‘ i • • • ' 1 1 > "‘ '1' 11 14*414 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40

31130A.D GCMS0103.M Wed Feb 06 09:22:47 2002 Page 3

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