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GCMS sample analysis results, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.

NYC-WTC_000019130–000019152

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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Scanned page image, NYC-WTC_000019141
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclohexanol, 4-methyl- Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

18.16 0.59 ug/,1 222372 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexanol, 4-methyl- 114 C7H140 000589-91-3 11 2 2-Propanones, 1-(1-methylethoxy)- 116 C6H12O2 042781-12-4 10 3 2-Propenenitrile, 3-(acetyl oxy)- 111 C5H5NO2 014268-54-3 9 4 2,4,4-Trimethylbut-2-enolide 126 C7H10O2 004182-41-6 9 Abundance Scan 1428 (18.156 mln): 30256.D (-) m/ z 43.05 100.00% 43 57 73 5000 111 95 TTTfr I 1 I ‘‘ • ' 1 „ 127 146 17.80 18.00 18.20 18.40 -tm 83 201 T.!,... 1 .. ||.... |. fl 11....!,... 11.. 111... | >... |.... | m/z 57.00 66.90% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160 170 180190200 Abundance #64161: Cyclohexanol. 4-methyl- 57

,1 — PAPeer, 111s 5000 17.80 18.00 18.20 18.40 81 m/z 73.00 54.21% 70 96 __i .nIB9p—mnmpnpgTT _Trrrr 114 I’**’I’IBSIUBIOD—AA*’*AAL’’’H miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #3286; 2-Propanone. 1-(1-methylethoxy)- 43

17.80 18.00 18.20 18.40 5000 m/z 111.10 41.26% 27 58 73 . . । . . . . । । i . । i'. . . , । I* pTTrpTTTpn-rTpTTTpTTTpTTTp-rrrpTTTpTTTJTTTTpTTTprrrj^^

m/z-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150 160 170180190200 #2407: 2-Propenenitrile, 3-(acetyloxy)- .. 1.,I,.

43 111 17.80 18.00 18.20 18.40 ‘ ‘ ' m/z 69.10 26.55% 5000-

15 77 1111 l'i 111 H 111 n 11 52...... 1.... 94 111'l i H11111111611 > 111111 . I.... l'l... J.... J.... 1.... 1...»IJ.... J.... 1 , ! . , I . l I"I -r ! I’l ri । । i । i i j i miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 17.80 18.00 18.20 18.40

30256.D GCMS1126.M Wed Jan 02 10:24:30 2002 Page 5 NYC-WTC_000019141

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NYC-WTC_000019141Source: NYC Law Department, mirrored locally

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