Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
NYC-WTC_000019130–000019152Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30256.D vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.
20.28 4.89 ug/1 1839800 Acenaphthene-dl0 20.56
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 40 2 3-Isopropoxy- 1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OS13 000000-00-0 16 4 Octadec oic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10 Abundance 73 Sean 1659 (20.276 mln): 30256.D (-) m/z 72.95 100.00%
5000 147 281 327 .....ly....... 20.00 20.20 20.40 20.60 45 191 2?1 251 Pi । TTT . 355,383 415, , । , , , , । ■ , , , । , 117 0-— । -I m/z 147.00 35.75% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 ................. ............................. 5000 20.00 20.20 20.40 20.60 369 m/z 281.00 32.90% , 207 249 338 J.................. —TI ----- miz-s 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-Isopropoxy-1,1,1.7.7,7-hexamethyl-3,5,5-tris(trim 73
20.00 20.20 20.40 20.60 5000 m/z 326.90 13.36% 147 221 281 327 415 519 561 miz-> 50 100 150 200 250 300 350 ‘ ' 400 450 ‘ ‘ 500 550 ‘ Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 20.00 20.20 20.40 20.60 m/z 282.00 8.98% 327 5000 237 45 147 | 172 212 [ i[ , i___________________________ ’ 4/s*)/At/Jf44 Jsu • • i ' ■ ■ ’ i ■ • ■ ' i • ■ ■ ‘ i ■ 1 1 ■ j • ■ ■ 1 i ■ ■ 1 • 1***1. 1 ‘ 1 1 ’ J I * m/z—> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30256.D GCMS1126.M Wed Jan 02 10:24:35 2002 Page 6
NYC-WTC_000019142
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NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000019035
Fragment of a GCMS document collection from December 2001 with minimal visible text.
Filed in the same folder
NYC-WTC_000019036
Record of Method 502 GCMS analysis data and quality control parameters for samples analyzed in December 2001.
Filed in the same folder
NYC-WTC_000019040
Calibration report for gas chromatography-mass spectrometry analysis of nitrosamines and chlorinated benzenes conducted on December 22, 2001.
Filed in the same folder
NYC-WTC_000019044
Reference analysis report for gas chromatography-mass spectrometry quantification of volatile organic compounds conducted on December 29, 2001.
Filed in the same folder
NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
Filed in the same folder