Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
NYC-WTC_000018248–000018261Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30984.D Vial: 38 Acq On 2 Jan 2002 12:47 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 4-Amino-5-imidazole carboxamid Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
17.45 3.10 ug/1 1144590 Naphthalene-d8 15.27
Hit# Of 5 Tentative ID MW Mol Form CAS# Qual
l 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 32 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 16 3 1,1,1,5 7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 4 Silane, Abundance ■...... [1,2,3-benzenetriyltris(oxy342C15H3003S13 Scan 1351 (17.450 min): 30984.D (-) m/ z 017864-23-2 9 72.9,5 100.00% 73
5000 341 45 147 I ‘ 1** 17.20 1740 17.60 17,80 ' ’ I ‘ ‘
I 117 L 179.. 207225 251 281 311 L [ 397 429 “ i “' ‘ i ‘ mpgngammmmeg—meTmepmepunmmeumppgp 14441734 m/z 341.0p 26.71% m/z~> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73
327 5000 ‘ ■ i ‘ • • ■ i ■ ■ 237 17.20 17.40 17.60 17.80 45 m/z 147.00 13.78% —u0—I u0—21—9“"B——147 Om—172 212 । $5 mmmmmmmmmmm EmmOTTOWTg m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337: 2H-1 4-Senzodiazepin-2-ono. 7-chloro-1 3-dihydro-5- 73 341 ■ 1 i ‘ 1 ...................... 16b I I J » . 17.20 17.40 17.60 17.80 5000 m/z 342.0.0 9.14% 45 | 91 ! | 116 146 227 269 315, j DTpppgmpp ■" • i ■ ■' ■ I m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 ....................... ....................... Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 17.20 17.40 17.60 17.80 m/z 325.0p 9.09% 147 5000 267 355 429 45 207 .. I, 11 n 111 n 11 n 11 n ............... I I ...... ‘[2199091—0090000010301333831 1111 111111111111 ri pi 11 TTTTTTTTTTpTTTpTrrp- , ...... 7 y............ miz-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17'40 17.60 17.80
30984.D GCMS1126.M Wed Jan 23 08:53:35 2002 Page 4
NYC-WTC_000018258
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NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018142
Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016783
GCMS analysis of environmental sample AD30118 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder