GCMS analysis results for sample AE12674, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12674 conducted on June 6, 2002.

NYC-WTC_000015006–000015015

Folder label: “GCMS X 5/30/02 A 6/1/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\MAY3 102\12674.D Vial: 19 Acq On 1 Jun 2002 5:42 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) .. Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Fluorononane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.11 0.60 ug/1 39947 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Fluorononane 146 C9H19F 000463-18-3 10 2 Hexane/ 2-methyl- 100 C7H16 000591-76-4 9 3 Ethanol, 2,2,2 -tri chi oro- 148 C2H3C130 000115-20-8 9 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 7 Abundance Scan 334 (8.109 min): 12674.D (-) m/z 42.90 100.00% 43

5000

97 127 "’’7*’47*’’I ItTTi i . ■ । । 36 63 85 119 | 7.80 8.00 8.20 8.40

miz-> .... I. 51 20 30 40 50 60 1 ■ ■ i ■ ■' ■ i ■ • ■ ■ i ■ 70 80 L ‘1 I ’ ’’I* 90 .Illi................. * ■■i■■ 1 ■। * ** ■ । '■ •11 * * 100 110 120 130 140 150 m/z 42.00 26.70% Abundance #8922:1-Fluorononane 43

5000 27 56 70 84 ' 7.80 8.00 8.20 8.40 ' ' ' 97 m/z 126.85 21.82% 11 ■ ■ • ■ i ' ■ i | ■ • i > ■ 1 TIun .. 1 ■ 11'1 ■■i■•■•i■■1‘1111' 11111111 mtz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #63433: Hexane, 2-methyl- 43 1 7.80 8.00 8.20 8.40 5000 m/z 97.00 21.52 57 85 27 ...... 1 _ Il *upur TIBBBu71—Buhur 100 I'' " I " '' I ‘ ‘‘ I ‘' 11 ■ ‘' I " '' I ‘' mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: Ethanol, 2,2,2-trichloro- ■ ■ ‘ i ■ ■ ■ 1 i ‘ ■ 1 ‘ i • ' ■ ‘ i ‘ ' i 31 7.80 8.00 8.20 8.40 m/z 124.90 19.79? 5000 49 77 113 61 . .... . n/z—> ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i' ■ 20 30 40 50 ।_____ I'111 r‘'1' 111 60 70 80 90 uu i*• ** । i ■ ■ ■ ■ । ■ ■ ■ • । 100 110 120 130 140 150 150 ■ ■ ' i ■ ■ ■ * i ■ 7.80 8.00 ' ‘ 1 ' 1 ' ' I ' 1 ' ' I 8.20 8.40

12674.D GCMS0531.M Mon Jun 03 11:45:07 2002 Page 2

NYC-WTC_000015014

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NYC-WTC_000015014Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE12672, June 2002 · Box DEP Box 15

NYC-WTC_000014943

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12672 conducted on June 6, 2002.

1 shared topics · Same agency, volume and box · similarity 0.998