GCMS analysis results for sample AE12674, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY3102\12674.D Vial: 19 Acq On 1 Jun 2002 5:42 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) .2 Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.06 1.28 ug/1 85181 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 59 2 Acetidacid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 28 3 Acetone 58 C3H60 000067-64-1 9 4 Morpholine, 4-methyl- Abundance __________ 101 C5H11NO Scan 329 (8.063 min): 12674.D (-) 000109-02-4 9 m/z 42.9.0 100.00% 43

59 5000

101 3147’1’473411 IUBTT’l i . 7.80 8.00 8.20 8.40 -......... 49 1 83 m/z 59.00 52.17% I ■ • ■ ■ i • ■ ■ ‘ i ■ ■ ■ ■ i ■ ■ ■ ‘ i 1 ■ • ■ i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 nBmmmRT 59 7.80 8.00 8.20 8.40 m/z 58.00 18.21% 15 31 — 83 101 | ----- 13 i T —————— miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 43 -1 t I t t I t l l . , AAA,

7.80 8.00 8.20 8.40 5000 57 m/z 101.05 17.98% 101 15 27 । T ' i 1 ■ mfz~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 m/z 41.00 7.29% 5000 15 58 27

m/z—> --PP 10 20 30 40 1 ■ l ■ ‘ 50 i ■ ‘ ■ ■ i ■ ■ ■ ‘ i ■ ‘ • ■ i ■ ■ 1 1 i ■ • ' ‘ i ■ 1 PMMMAAA 60 70 80 90 100 110 7.80 8.00 8.20 8.40

12674.D GCMS0531.M Mon Jun 03 11:45:06 2002 Page 1

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