GCMS analysis comments for sample AD28598, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\28651.D vial: 49 Acq On : 30 Nov 2001 2:41 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************* ********** * ** *** * * ******************** Peak Number 3 Dodecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 28.35 1.20 ug/1 342627 Phenanthrene-dl0 25.00 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Dodecane 170 C12H26 000112-40-3 64 2 Pentadecane 212 C15H32 000629-62-9 58 3 Heptadecane 240 C17H36 000629-78-7 53 4 Octadecane, 1-chloro-_______________ 288 C18H37C1 _____ 003386-33-2 52 Abundance Scan 2539 (28.350 min): 28651 D (-) m/z 57.00 100.00% 57 43 71 5000 91

28.00 28.20 28.40 28.60 4.1 l 81 L’I 125135,147,161 JTC 4—1 203 724 . m/z43.05 77.66% miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #68253: Dodecane 43 57

71 5000 85 28.00 28.20 28,40 28.60 m/z 71.00 61.90% 98 112 170 ■ ' i ■ ■ I 11 — 1 — 126 141 n-r- 1 miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #26001: Pentadecane 57 43 71 • i i i i ■ 28.00 28.20 28.40 28.60 5000 85 m/z 41.0.5 51.15%

99 44,

mz—> ■ 1 i ■ ■ ■ 1 । 1 40 60 +— 80 1113 127......... 168.......... 212 120 100 160 140 180 200 220 240 Abundance #71191: Heptadecane 43 57 28.00 28.20 28.40 28.60 m/z 55.00 48.22% 71 5000 85

— — 99 113 127 141.............................. 240 l ■ .80, . 100 1 ' i 1 ■ ■ ’I■ ■। । । ।। ■ 1 1 i ■ ■■ •I 11 1 1 I 1 1 1 1 I ' ' ' 1 I '1 Tl/z-> 40 I60 120 140 160 180 200 220 240 28.00 28.20 28.40 28.60

28651.D GCMS1126.M Fri Nov 30 16:42:56 2001 Page 3

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