GCMS analysis comments for sample AD28598, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\28651.D Vial: 49 Acq On : 30 NOV 2001 2:41 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 125693 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 37 3 Benzof razan, 5-methoxy- 150 C7H6N202 004413-48-3 9 4 Vanill n 152 C8H803 000121-33-5 9 Abundance Scan 711 (11.569 min): 28651 .D (-) m/z 149.90 100.00% 150

5000 115 52 78 1 ——

n/z-> 20 40 I . 64 PP4 + 1 —Hm 30 40 11 87 - 50 60 70 80 90 r ioo' 718720 730 140 788 160 11.20 11.40 11.60 11.80 m/z 151.90 63.86% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 52 78 11.20 11.40 11.60 11.80 11 m/z 114.90 37.74% —— miz-> 20 30 35 40 50 ‘I" 60 70 80 90 L 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- KO ---------- 115 1120 11.40 11,60 11.80 5000 52 78 m/z 78.05 19.31%

35 87

mlz-> 20 1 TtI"E11111171 30 40 50 1 ’ | 1 1 • r| । ! 60 1 i11'' 11'' 11 ■' ■ ■ i ■ ■ 70 80 90 100 110 120 130 140 150 160 I— Abundance #9639: Benzofurazan, 5-methoxy- 150 11.20 1140 11.60 11.80 ' m/z 52.00 . 16.40%

5000 120 77 65

20 —........... '

30 40 50 60 i -mmp >1 90 70 105 80 90 100 110 120 130 140 150 160 111'f ‘11 • • • ' i' I T T 11.20 11.40 11.60 11.80 tit

28651.D GCMS1126.M Fri Nov 30 16:42:53 2001 Page 2

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