GCMS analysis comments for sample AD28596, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28598 .D vial: 47 Acq On : 30 Nov 2001 8:09 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.51 ug/1 114905 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene- 1,2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 4 -Amino 2- chlorobenzonitrile 152 C7H5C1N21 020925-27-3 10 4 Vanillin 152 C8H803 000121-33-5 9 Abundance 7 Scan 710 (11.560 min): 28598.D (-) m/z 149.90 100.00% 150

5000 115 78 ■ । i r i i ] ■ ■ TTI— i TIT I i i | i 52 11.20 11.40 11.60 11.80

mz-> 38 -IHH r -- i ■' • ■ l 87 103 30 40 50 60 70 80 90 100 110 120 63 + 130 140 — 150 160 m/z 151.90 64.71% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 11.40 11.60 11.80 52 m/z 114.90 . 37.93% 35 — ■' i ■ ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro- 110

115 11.20 11.40 11.60 11.80 5000 52 78 m/z 77.95 _ 21.24%

35 87 |______ ' ■ i 1 ' ■ ' i 1 ■ ■ ' I • • i ■1 ■ ■ i11 I t-p-r-rr-p 1911 I''''I'' I 1 mlz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10110: 4-Amino-2-chlorobenzonitrile "b T 152 11.20 11.40 11.60 11.80 m/z 52.00 15.22% 5000

90 117 125 63 76 ’ ■ i ■ ■ ■ ■ i ' ■ '' i ' ■ ■ ■ i1 ' ■ ■ i ■ ■1 ■ 1 1 ........... 4— ........ PP ‘i T T T I’ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28598.D GCMS1126.M Fri Nov 30 15:32:49 2001 Page 1

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