GCMS calibration data sheet, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC3101 \LBA.D Vial: 5 Acq On : 31 Dec 2001 2:51 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Octadecane, 1-chloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

28.34 0.41 ug/1 103883 Phenanthrene-dl0 24.98

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane, 1-chloro- 288 C18H37C1 003386-33-2 2 Hexadecane, 1-chloro- 260 C16H33C1 004860-03-1 87 3 Tetracontane, 3,5,24-trimethyl- 605 C43H88 055162-61-3 78 4 Hexatriacontane 507 C36H74 000630-06-8 72 Abundance 57 Scan 2538 (28.343 mln): LBA.D (-) m/ z 57.00 100.00%

5000 91

28.00 28.20 28.40 28.60 ' T’ k1119, , . . . 207 . . . ...... .... ..... . n rl . . | i j. I I I | I ... j | < ...j | J . . m/z 43.05 95.37% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40870: Octadecane, 1-chloro- 57

5000 T T T T ‘I 91 28.00 28.20 28.40 28.60 m/z 41.05 71.16% 1119, 261288 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #35935: Hexadecane. 1-chioro- 57 1 ■ i ■ • ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i • ■ ■ ■ i 28.00 28.20 28.40 28.60 91 m/z 71.00 56.66% 5000

- miz-> 50 100 150 200 250 ‘ ' 300 350 400 ' 450 500 550 Abundance #60914: Tetracontane, 3,5,24-trimethyl- ' 1 i 1 1 1 ■ 1 1 T T TI 57 28.00 28.20 28.40 28.60 —

5000 85

' ‘ i ■ 1 11’11,141 ... 238 ........ ■.... 505 547 ■ 1 i ‘ ■ i 1 ‘ 1 • i • • ■ • i ■ • ■ ‘ i miz-> 50 100 150 200 250 300 350 400 450 500 550 28.00 28.20 28.40 28.60

LBA.D GCMS1126.M Wed Jan 16 08:29:31 2002 Page 3

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