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GCMS calibration data sheet, Dec 2001

Machine-extracted title · confidence 95%

Document showing calibration results for GCMS analysis of volatile organic compounds on December 31, 2001.

NYC-WTC_000017883–000017893

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC3101\LBA.D Vial: 5 Acq On : 31 Dec 2001 2:51 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Octacosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

30.62 0.37 ug/1 65156 Chrysene-dl2 33.03

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Octacosane 394 C28H58 000630-02-4 52 2 Hexadecane, 2,6,10,14-tetramethyl- 282 C20H42 000638-36-8 50 3 Tridecane, 2,2,4,10,12,12-hexamethy 394 C28H58 003035-75-4 50 4 Tetradecane, 1-bromo- 276 C14H29Br 000112-71-0 43 Abundance Scan 2786 (30.620 mln): LBA.D (-) m/z 57.00 100.00% 57

5000 85 AWAA J 11 113 u 141 34+4---------++++++ MMHH .... 208 Pijn 30.20 30.40 30.60 30.80 31.00 m/z 43.05 87.24% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #53457: Octacosane 57 AAW) WAAA 5000 85 30.20 30.40 30.60 30.80 31.00 113 m/z 55.00 63.85% 1 J ] 141 183 267 394 40 80 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 ‘ miz-> Abundance #39868: Hexadecane, 2.6.10,14-tetramethyl- MwAwd WAAyw 57 T TT T 30.20 30.40 30.60 30.80 31.00 5000 85 m/z 71.10 55.07% 113 [ i , m/z-> U1 169 197 252 282 II... JI(. K. i I... I!J......... J> 1111111111-r 11J > 1 ■> 111111 ■' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 AAJ WAWAA Abundance #53459: Tridecane, 2,2,4,10,12.12-hexamethyl-7-(3,5,5-trime 57 30.20 30.40 30.60 30.80 31.00 m/z 41.05 51.14% I 5000 wsrW/ yuM । 85 „ 113 141 < t । i i > 4 । i i > i । t > i i224 ,mmmmpn 281 336 11+1’44 । i i i k। ir|ii jii i i।>i>i।iiii।iiii|11|Ij l 1 4 | | r ii

m/z-> 40 80 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 30.20 30.40 30.60 30.80 31.00

LBA.D GCMS1126.M Wed Jan 16 08:29:35 2002 Page 4

NYC-WTC_000017892

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NYC-WTC_000017892Source: NYC Law Department, mirrored locally

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