GC/MS analysis results, sample AD22919, October 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT0201\22919.D Vial; 9 Acq On ; 2 Oct 2001 9:56 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octacosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 32.76 0.64 ug/1 81467 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octacosane 394 C28H58 000630-02-4 91 2 Heptadecane 240 C17H36 000629-78-7 91 3 Docosane 310 C22H46 000629-97-0 91 4 Heneicosane 296 C21H44 000629-94-7 91‘ Abundance Scan 3019 (32.760 min); 22919.D (-) m/z SYTOO 100.00% 57 J 85

u 5000 4 —ry I ft . I , . 5 1 |Tm । . . i~|*f

208 281 _3Z40_JZ60_3Z80^10g__ I'''' I' I'' I'' ’' I'''' I'''' I'''' I ‘' I''' ’ I ‘' m/z 71.10 73.22% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74211: Octacosane 43

71 5000 32.40 32.60 32.80 33.00 tn/z 43.00 66.30% I I , 127 155 183 211 364 I " " I " ‘ • I' • " I “ • ‘ I ' I''' ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #32063; Heptadecane 57

85 32.40 32.60 32.80 33.00 5000 m/z 85.05 51.90%

„ 1 .... 196. 2^ '' I'' I . il I I II k I I I I Ti I I H I I I I I I I I I I I I I I I I I I I I I p TTrtTTTTTTTTTp-TTTpTT-rYTTTT^^ TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 <\bundance #44318; Docosane 57 32.40 32.60 32.80 33.00 m/z 41705 30761% 5000 85 J

jLuTkjkx I I 11 I pl I I I I I 11 I I I I I J I I i I j n I I I 266 I' ‘ ' I 310 iVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 32.40 32.60 32.80 33.00

22919.D NP091101.M Thu Oct 04 10:03:36 2001 Page 7

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