GCMS analysis results for sample AE10517, May 2002

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Data File : C:\HPCHEM\l\DATA\MAY1002\10517.D vial: 40 Acq On : 12 May 2002 4:06 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 4 l-Dotriacontanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 28.80 0.51 ug/1 61902 Phenanthrene-dl0 25.55 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Dotriacontanol 467 C32H660 006624-79-9 91 2 1-Hexadecanol 242 C16H340 036653-82-4 90 3 1-Octadecanol 270 C18H380 000112-92-5 90 4 1-Octadecene 252 C18H36 000112-88-9 76 Abundance Scan 2593 (28.802 min): 10517.D (-) m/z 43.15 100.00% 43 83

5000 111 I I 1 I I I I ’ ’ I I I I I I I I I I ’ I I I

m/z-> lLi 50 118 100 150 200 250 300 350 400 450 28.40 28.60 28.80 29.00 29.20 m/z 55.05 89.58% Abundance #57795:1-Dotriacontanol 57

83 5000 28.40 28.60 28.80 29.00 29.20 111 m/ z 57.05 84.11%

L — 1138 196 Li[s TI■ 420 448 ■ > ■ । ■ m/z-> 50 100 150 200 250 300 350 400i 450 Abundance #71249:1-Hexadecanol 55 83 28.40 28.60 28.80 29.00 29.20 5000 m/ z 83.10 79.21% 111

TT 11139, , 196 224 1 1 I ' i ' ■ i ' ■ ■ ■ ■ i ■ LI-' TIl m/z-> 50 100 150 200 250 300 350 400 450 Abundance #72029:1-Octadecanol M., M ' s ' 1 ' ■ I ’ ■ ' ' I ' ‘ 43 83 28.40 28.60 28.80 29.00 29.20 m/ Z 69.05 72.23% 5000 111

224 252 IAA/MA _____________ rk' 1 l 1 '' ' 1 I 1 TT । i । ll j i rt ’ । i i i i ] । i—।—।—।—i—r m/z-> 50 100 150 200 250 300 350 400 450 28.40 28.60 28.80 29.00 29.20

10517.D GCMS0510.M Thu May 16 15:10:31 2002 Page 4

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