GCMS analysis results for sample AE10517, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAY1002\10517.D Vial: 40 Acq On : 12 May 2002 4:06 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 1-Octadecene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

31.14 22.47 ug/1 1771450 Chrysene-dl2 33.61

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octadecene 252 C18H36 000112-88-9 98 2Phosphonicacid, dioctadecyl ester 587 C36H75O3P 019047-85-9 76 3 5-Eicosene, (E) - 280 C20H40 074685-30-6 76 4 1-Docosene 308 C22H44 001599-67-3 76 Abundance Scan 2848 (31.138 min): 10517.D (-) m/z 55.10 100.00% 55

5000 73 4 97 111 127 . y1,1।1111।' II I, mlz-> lu 1 l 141155169183197211225 252267281295 324 m/z 43.15 TTIud trr Tt ! T[ li ili । IT । r' | । i r i । । r । । । । । । r । । । । । । i i । i । । । । । । । । । । j । i । i । । । । । । i i । 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.80 31.00 31.20 31.40_____ 55.45% Abundance #71503:1-Octadecene 55

83 97 5000 ..... J.... I i | i । । । | r i t 1 | | I | | | ri I I [ll

30.80 31.00 31.20 31.40 111 ■m/z 57.10 48.21%

‘ "I" i ■1 1111 125 252 1111')1111111111111 r t1 ■11111111111111 ‘ 111 >> 11 [' ।11111 A m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #60683: Phosphonic acid, dioctadecyl ester 55 69 83 97 TlnnT 30.80 31.00 31.20 31.40 5000 m/ Z 73.10 46.19% 111 136 ' 1 1 1 ' 11 ‘II “ i i । i i । i । i i । । । । । । । । i i i i । i i i i । i । । i । । । i r["i । । । । । । । r pi ti i t r j i । i i

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #39520:5-Eicosene, (E)- ..................).................... 1 ' i 11 1 1 i ■1 ' 1 n 1 1 ■ i ‘ 11 1 i 1 55 30.80 31.00 31.20 31.40 m/ z 83.15 42.85% 83 97 5000

111

i ■ ■1 r । , 125,39 252 280 1*01001002/11010011000100000710— i । । । i । । [ I I I I C "i r i | I i I I [ I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.80 31.00 31.20 31.40

10517.D GCMS0510.M Thu May 16 15:10:32 2002 Page 5

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